10β-Hydroxy-1,4-estradiene-3,17-dione
Bieri, J. H. (Universität Zürich. Organisch-chemisches Institut)
Prewo, R. (Universität Zürich. Organisch-chemisches Institut)
Briansó, José Luis (Universitat Autònoma de Barcelona. Departament de Geologia)
Piniella, J. Francesc (Joan Francesc) (Universitat Autònoma de Barcelona. Departament de Geologia)
Date: |
1985 |
Abstract: |
C18H22=3 Mr=286. 4, orthorhombic, P212121, a=7. 014(2), b=12. 176(4), c=17. 648(4)A, V=1507. 2 A3, Z=4, Dx=1. 26 Mg m-3m (Mo Ka)=0. 71069 A, µ=0. 079 mm-1m F(000)=616, T ca 130 K, R=0. 109 for all 2506 unique reflections within -1sinO=0. 70 A-1; the absolute configuration was not determined. The relative stereochemistry at C(10) is established. The unsaturated ring is essentially planar; the two central rings are in the chair conformation and the five-membered ring adopts the envelope conformation. |
Rights: |
Tots els drets reservats. |
Language: |
Anglès |
Document: |
Article ; Versió publicada |
Subject: |
Cristal·lografia ;
Crystallography |
Published in: |
Acta Crystallographica. Section C: Crystal Structure Communications, Vol. 41, Issue 10 (October 1985) , p. 1530-1532, ISSN 1600-5759 |
DOI: 10.1107/S0108270185008435
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Record created 2008-07-29, last modified 2023-10-03