cd3039409a3e8715d6ada47af0813a1c pmc_28773602.pdf 744ef728774cac3cc8185a2c2591956c6e1bc588 pmc_28773602.pdf 0eb897b1bbc4a323276fec40cca0ffbe381275d6ada13007cb8d2af32a141f9d pmc_28773602.pdf Title: Synthesis of Mixed Cu/Ce Oxide Nanoparticles by the Oil-in-Water Microemulsion Reaction Method Subject: Cerium oxide and mixed Cu/Ce oxide nanoparticles were prepared by the oil-in-water (O/W) microemulsion reaction method in mild conditions. The Cu/Ce molar ratio was varied between 0/100 and 50/50. According to X-ray diffraction (XRD), below 30/70 Cu/Ce molar ratio, the materials presented a single phase consistent with cubic fluorite CeO2. However, above Cu/Ce molar ratio 30/70, an excess monoclinic CuO phase in coexistence with the predominant Cu/Ce mixed oxide was detected by XRD and High-Resolution Transmission Electron Microscopy (HRTEM). Raman spectroscopy showed that oxygen vacancies increased significantly as the Cu content was increased. Band gap (Eg) was investigated as a function of the Cu/Ce molar ratio, resulting in values from 2.91 eV for CeO2 to 2.32 eV for the mixed oxide with 30/70 Cu/Ce molar ratio. These results indicate that below 30/70 Cu/Ce molar ratio, Cu2+ is at least partially incorporated into the ceria lattice and very well dispersed in general. In addition, the photodegradation of Indigo Carmine dye under visible light irradiation was explored for selected samples; it was shown that these materials can remove such contaminants, either by adsorption and/or photodegradation. The results obtained will encourage investigation into the optical and photocatalytic properties of these mixed oxides, for widening their potential applications. Keywords: mixed oxide nanoparticles; microemulsion; nanoreactor; CeO2 NPs; CuO NPs Author: Kelly Pemartin-Biernath, Andrea V. Vela-González, Maira B. Moreno-Trejo, César Leyva-Porras, Iván E. Castañeda-Reyna, Isaías Juárez-Ramírez, Conxita Solans and Margarita Sánchez-Domínguez Creator: LaTeX with hyperref package Producer: pdfTeX-1.40.15 CreationDate: Thu Jun 16 08:36:35 2016 CEST ModDate: Thu Jun 16 08:36:35 2016 CEST Tagged: no UserProperties: no Suspects: no Form: none JavaScript: no Pages: 21 Encrypted: no Page size: 595.276 x 841.89 pts (A4) Page rot: 0 File size: 20834889 bytes Optimized: no PDF version: 1.5 name type encoding emb sub uni object ID ------------------------------------ ----------------- ---------------- --- --- --- --------- NFZNXD+URWPalladioL-Ital Type 1 Custom yes yes no 108 0 ILAFDF+URWPalladioL-Bold Type 1 Custom yes yes no 109 0 OCBAZT+URWPalladioL-Roma Type 1 Custom yes yes no 110 0 YOTXCC+TimesNewRomanPS-BoldItalicMT Type 1C WinAnsi yes yes no 115 0 ZFDDWN+TeX-matha8 Type 1 Builtin yes yes no 160 0 LTQZXI+TeX-matha7 Type 1 Builtin yes yes no 190 0 ENANDN+EURM7 Type 1 Builtin yes yes no 207 0 GQCTVQ+TeX-matha10 Type 1 Builtin yes yes no 208 0 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LastModified: 2018-02-06 08:59:29 CET Size: 20834889 Format: PDF Version: 1.5 Status: Well-Formed and valid SignatureMatches: PDF-hul MIMEtype: application/pdf PDFMetadata: Objects: 0 FreeObjects: 1 IncrementalUpdates: 0 DocumentCatalog: ViewerPreferences: HideToolbar: false HideMenubar: false HideWindowUI: false FitWindow: true CenterWindow: false DisplayDocTitle: false NonFullScreenPageMode: UseNone Direction: L2R ViewArea: CropBox ViewClip: CropBox PrintArea: CropBox PageClip: CropBox PageLayout: SinglePage PageMode: UseNone Outlines: Item: Title: ぉのぴひはつふっぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸲ Item: Title: げづびふぬぴびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮ㄩ‾㸊⡜㌷㙜㌷㝜〰きどっひはづねふぬびどはのぜ〴ぜ〰うはひねふぬちぴどはのぜ〴ぜ〰ちのつぜ〴ぜ〰こべのぴとづびどびぜ〴ぜ〰はてぜ〴ぜ〰ぃふ〯ぃづぜ〴ぜ〰ぎちのはばちひぴどっぬづびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㈩‾㸊⡜㌷㙜㌷㝜〰ぃとちひちっぴづひどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぃふ〯ぃづぜ〴ぜ〰くへどつづぜ〴ぜ〰ぎぐびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獵扳散瑩潮⸲⸲⸱ Children: Item: Title: きどっひはづねふぬびどはのぜ〴ぜ〰うはひねふぬちぴどはのぜ〴ぜ〰ちのつぜ〴ぜ〰こべのぴとづびどびぜ〴ぜ〰はてぜ〴ぜ〰ぃふ〯ぃづぜ〴ぜ〰ぎちのはばちひぴどっぬづびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㈩‾㸊⡜㌷㙜㌷㝜〰ぃとちひちっぴづひどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぃふ〯ぃづぜ〴ぜ〰くへどつづぜ〴ぜ〰ぎぐびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獵扳散瑩潮⸲⸲⸱ Item: Title: ぃとちひちっぴづひどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぃふ〯ぃづぜ〴ぜ〰くへどつづぜ〴ぜ〰ぎぐびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獵扳散瑩潮⸲⸲⸱ Children: Item: Title: えどでとぜ〴ぜ〰げづびはぬふぴどはのぜ〴ぜ〰ごひちのびねどびびどはのぜ〴ぜ〰ぅぬづっぴひはのぜ〴ぜ〰きどっひはびっはばべぜ〴ぜ〰ぜ〵ぜ〰えげごぅきぜ〵ㅜ〰ぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獵扳散瑩潮⸲⸲⸲ Item: Title: じ〭ひちべぜ〴ぜ〰いどててひちっぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獵扳散瑩潮⸲⸲⸳ Item: Title: げちねちのぜ〴ぜ〰こばづっぴひはびっはばべぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㌩‾㸊⡜㌷㙜㌷㝜〰きちでのづぴどっぜ〴ぜ〰ぐひはばづひぴどづびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㐩‾㸊⡜㌷㙜㌷㝜〰くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰いづでひちつちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぉのつどではぜ〴ぜ〰ぃちひねどのづぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸳ Item: Title: きちでのづぴどっぜ〴ぜ〰ぐひはばづひぴどづびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㐩‾㸊⡜㌷㙜㌷㝜〰くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰いづでひちつちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぉのつどではぜ〴ぜ〰ぃちひねどのづぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸳ Item: Title: くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰いづでひちつちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぉのつどではぜ〴ぜ〰ぃちひねどのづぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸳ Item: Title: いどびっふびびどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮ㄩ‾㸊⡜㌷㙜㌷㝜〰きどっひはづねふぬびどはのぜ〴ぜ〰うはひねちぴどはのぜ〴ぜ〰ちのつぜ〴ぜ〰ぐちひぴどっぬづぜ〴ぜ〰こべのぴとづびどびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㈩‾㸊⡜㌷㙜㌷㝜〰ぃとちひちっぴづひどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぃふ〯ぃづぜ〴ぜ〰くへどつづぜ〴ぜ〰ぎちのはばちひぴどっぬづびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㌩‾㸊⡜㌷㙜㌷㝜〰きちでのづぴどっぜ〴ぜ〰ぐひはばづひぴどづびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㐩‾㸊⡜㌷㙜㌷㝜〰くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰ぁっぴどぶどぴべぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Children: Item: Title: きどっひはづねふぬびどはのぜ〴ぜ〰うはひねちぴどはのぜ〴ぜ〰ちのつぜ〴ぜ〰ぐちひぴどっぬづぜ〴ぜ〰こべのぴとづびどびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㈩‾㸊⡜㌷㙜㌷㝜〰ぃとちひちっぴづひどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぃふ〯ぃづぜ〴ぜ〰くへどつづぜ〴ぜ〰ぎちのはばちひぴどっぬづびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㌩‾㸊⡜㌷㙜㌷㝜〰きちでのづぴどっぜ〴ぜ〰ぐひはばづひぴどづびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㐩‾㸊⡜㌷㙜㌷㝜〰くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰ぁっぴどぶどぴべぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Item: Title: ぃとちひちっぴづひどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぃふ〯ぃづぜ〴ぜ〰くへどつづぜ〴ぜ〰ぎちのはばちひぴどっぬづびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㌩‾㸊⡜㌷㙜㌷㝜〰きちでのづぴどっぜ〴ぜ〰ぐひはばづひぴどづびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㐩‾㸊⡜㌷㙜㌷㝜〰くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰ぁっぴどぶどぴべぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Item: Title: きちでのづぴどっぜ〴ぜ〰ぐひはばづひぴどづびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㐩‾㸊⡜㌷㙜㌷㝜〰くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰ぁっぴどぶどぴべぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Item: Title: くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰ぁっぴどぶどぴべぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Item: Title: きちぴづひどちぬびぜ〴ぜ〰ちのつぜ〴ぜ〰きづぴとはつびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮ㄩ‾㸊⡜㌷㙜㌷㝜〰きちぴづひどちぬびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㈩‾㸊⡜㌷㙜㌷㝜〰ぐひづばちひちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぎぐびぜ〴ぜ〰ぢべぜ〴ぜ〰ぴとづぜ〴ぜ〰く〯しぜ〴ぜ〰きどっひはづねふぬびどはのぜ〴ぜ〰げづちっぴどはのぜ〴ぜ〰きづぴとはつぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㌩‾㸊⡜㌷㙜㌷㝜〰ぃとちひちっぴづひどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぎぐびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㐩‾㸊⡜㌷㙜㌷㝜〰きちでのづぴどっぜ〴ぜ〰ぐひはばづひぴどづび〬ぜ〴ぜ〰くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰ぐづひてはひねちのっづぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸵ Children: Item: Title: きちぴづひどちぬびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㈩‾㸊⡜㌷㙜㌷㝜〰ぐひづばちひちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぎぐびぜ〴ぜ〰ぢべぜ〴ぜ〰ぴとづぜ〴ぜ〰く〯しぜ〴ぜ〰きどっひはづねふぬびどはのぜ〴ぜ〰げづちっぴどはのぜ〴ぜ〰きづぴとはつぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㌩‾㸊⡜㌷㙜㌷㝜〰ぃとちひちっぴづひどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぎぐびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㐩‾㸊⡜㌷㙜㌷㝜〰きちでのづぴどっぜ〴ぜ〰ぐひはばづひぴどづび〬ぜ〴ぜ〰くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰ぐづひてはひねちのっづぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸵ Item: Title: ぐひづばちひちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぎぐびぜ〴ぜ〰ぢべぜ〴ぜ〰ぴとづぜ〴ぜ〰く〯しぜ〴ぜ〰きどっひはづねふぬびどはのぜ〴ぜ〰げづちっぴどはのぜ〴ぜ〰きづぴとはつぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㌩‾㸊⡜㌷㙜㌷㝜〰ぃとちひちっぴづひどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぎぐびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㐩‾㸊⡜㌷㙜㌷㝜〰きちでのづぴどっぜ〴ぜ〰ぐひはばづひぴどづび〬ぜ〴ぜ〰くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰ぐづひてはひねちのっづぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸵ Item: Title: ぃとちひちっぴづひどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぎぐびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㐩‾㸊⡜㌷㙜㌷㝜〰きちでのづぴどっぜ〴ぜ〰ぐひはばづひぴどづび〬ぜ〴ぜ〰くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰ぐづひてはひねちのっづぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸵ Item: Title: きちでのづぴどっぜ〴ぜ〰ぐひはばづひぴどづび〬ぜ〴ぜ〰くばぴどっちぬぜ〴ぜ〰ぐひはばづひぴどづびぜ〴ぜ〰ちのつぜ〴ぜ〰ぐとはぴはっちぴちぬべぴどっぜ〴ぜ〰ぐづひてはひねちのっづぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸵ Item: Title: ぃはのっぬふびどはのびぜ〴〩਼㰠⽓ 䝯呯 䐠嬸㘠〠删⽆楴䡝‾㸊㰼ਯ呹灥 偡来ਯ䍯湴敮瑳‱〵‰⁒ਯ剥獯畲捥猠㄰㐠〠刊⽍敤楡䉯砠嬰‰‵㤵⸲㜶‸㐱⸸㥝ਯ偡牥湴‱ㄱ‰⁒ਯ䅮湯瑳⁛‸㜠〠删㠹‰⁒‹ㄠ〠删㤲‰⁒‹㌠〠删㤴‰⁒‹㔠〠删㤶‰⁒‹㜠〠删㤸‰⁒‹㤠〠删㄰㌠〠删崊㸾਼㰊⽐牯摵捥爠⡇偌⁇桯獴獣物灴‹⸱〩ਯ䍲敡瑩潮䑡瑥
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