516b99862dc848e31ffae6515adcb4e2 pmc_28852090.pdf 0aae0caa0d032b8f2a0cb7e9375c8862784b9385 pmc_28852090.pdf 3ddc943ea616fb1a6ab8e5e532c18d702ee9d99d9376f0ee87977422d3683711 pmc_28852090.pdf Title: Synthesis and Characterization of PtTe2 Multi-Crystallite Nanoparticles using Organotellurium Nanocomposites Subject: Scientific Reports, doi:10.1038/s41598-017-10239-8 Keywords: Author: Javier Fernamp#x000E1;ndez-Lodeiro Creator: Springer Producer: iText® 5.3.5 ©2000-2012 1T3XT BVBA (AGPL-version) CreationDate: Mon Aug 21 11:19:08 2017 CEST ModDate: Fri Aug 25 10:43:05 2017 CEST Tagged: no UserProperties: no Suspects: no Form: AcroForm JavaScript: no Pages: 10 Encrypted: no Page size: 595.276 x 782.362 pts Page rot: 0 File size: 1779289 bytes Optimized: no PDF version: 1.4 name type encoding emb sub uni object ID ------------------------------------ ----------------- ---------------- --- --- --- --------- KGXBDD+Corbel CID TrueType Identity-H yes yes yes 328 0 MinionPro-It Type 1C Custom yes no yes 118 0 QEVDVD+Corbel-BoldItalic Type 1C WinAnsi yes yes yes 329 0 HEXMCU+Corbel-Bold2 Type 1C WinAnsi yes yes yes 203 0 VHKPBH+Corbel-Bold CID TrueType Identity-H yes yes yes 27 0 XKDQLU+Corbel2 Type 1C WinAnsi yes yes yes 28 0 MinionPro-Regular Type 1C Custom yes no yes 29 0 KHQMDD+TimesNewRomanPSMT Type 1C WinAnsi yes yes yes 330 0 HEXMCU+Corbel-Bold2 Type 1C WinAnsi yes yes yes 279 0 KGXBDD+Corbel CID TrueType Identity-H yes yes yes 398 0 XKDQLU+Corbel2 Type 1C WinAnsi yes yes yes 281 0 MyriadPro-It Type 1C WinAnsi yes no yes 282 0 MinionPro-Bold Type 1C Custom yes no yes 25 0 EuclidSymbol Type 1C Custom yes no yes 26 0 XKDQLU+Corbel2 Type 1C WinAnsi yes yes yes 278 0 KGXBDD+Corbel CID TrueType Identity-H yes yes yes 280 0 KGXBDD+Corbel CID TrueType Identity-H yes yes yes 294 0 AIMZTX+STIXGeneral-Regular Type 1C Custom yes yes yes 119 0 EuclidSymbol-Bold Type 1C Custom yes no yes 192 0 EuclidSymbol-Italic Type 1C Custom yes no yes 260 0 Jhove (Rel. 1.28.0, 2023-05-18) Date: 2024-02-08 02:46:07 CET RepresentationInformation: pmc_28852090.pdf ReportingModule: PDF-hul, Rel. 1.12.4 (2023-03-16) LastModified: 2018-02-08 07:51:00 CET Size: 1779289 Format: PDF Version: 1.4 Status: Well-Formed and valid SignatureMatches: PDF-hul MIMEtype: application/pdf PDFMetadata: Objects: 452 FreeObjects: 1 IncrementalUpdates: 0 DocumentCatalog: ViewerPreferences: HideToolbar: false HideMenubar: false HideWindowUI: false FitWindow: false CenterWindow: false DisplayDocTitle: false NonFullScreenPageMode: UseNone Direction: L2R ViewArea: CropBox ViewClip: CropBox PrintArea: CropBox PageClip: CropBox PageLayout: SinglePage PageMode: UseOutlines Language: EN Outlines: Item: Title: Synthesis and Characterization of PtTe2 Multi-Crystallite Nanoparticles using Organotellurium Nanocomposites Children: Item: Title: Results and Discussion Children: Item: Title: Synthesis and morphological characterization of organometallic Pt-Te NPs. Item: Title: Chemical characterization of organometallic Pt-Te NPs. Item: Title: Metal-ligand interaction during the reaction. Item: Title: Synthesis and characterization of PtTe2 multi-crystallite NPs. Item: Title: Methods Children: Item: Title: Synthesis of organometallic Pt-Te NPs. Item: Title: Reverse order of reagent addition (entry R4). Item: Title: Synthesis in the presence of CH2Cl2/acetonitrile mixture (entry R5). Item: Title: Synthesis of multi-crystallite NPs. Item: Title: Fourier transform ion cyclotron resonance mass spectrometry (FT-ICR MS) analysis. Item: Title: Transmission electron microscopy (TEM) analysis. Item: Title: Scanning electron microscopy (SEM). Item: Title: X-ray photoelectron spectroscopy (XPS). Item: Title: UV/Vis and FT-IR spectroscopy studies. Item: Title: Inductively coupled plasma (ICP) analysis. Item: Title: Elemental analysis. Item: Title: Thermogravimetric analysis. Item: Title: Conclusion Item: Title: Acknowledgements Item: Title: Figure 1 (a) Low magnification TEM (a,b,d,e) and SEM (c,f) images of different sizes of organometallic Pt-Te NPs obtained under higher initial reagent concentrations ([Pt(IV)] = 2. Item: Title: Figure 2 (a) STEM-HAADF image of a group of Pt-Te NPs and Te, Pt, C, O and Cl EDS elemental maps (1–6). Item: Title: Figure 3 XPS spectrum of organometallic Pt-Te NPs. Item: Title: Figure 4 TEM (a), and STEM (b) images of PtTe2 multi-crystallite NPs obtained after the annealing process, HRTEM images of isolated NPs showing lattice image fringes (c,d) and electron diffraction pattern obtained from a group of PtTe2 multi-crystallite N Item: Title: Table 1 Experimental reaction conditions ([Reagent] in n/L and %H2O in V/V). 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doi:10.1038/s41598-017-10239-8 Springer US Scientific Reports, doi:10.1038/s41598-017-10239-8 Synthesis and Characterization of PtTe2 Multi-Crystallite Nanoparticles using Organotellurium Nanocomposites Javier Fernamp#x000E1;ndez-Lodeiro Benito Rodramp#x000ED;guez-Gamp#x000F3;nzalez Fernando Novio Adriamp#x000E1;n Fernamp#x000E1;ndez-Lodeiro Daniel Ruiz-Molina Josamp#x000E9; Luis Capelo Alcindo A. dos Santos Carlos Lodeiro 10.1038/s41598-017-10239-8 http://dx.doi.org/10.1038/s41598-017-10239-8 journal Scientific Reports © 0, The Author(s) 2045-2322 10.1038/s41598-017-10239-8 Springer 2017-08-25T10:43:05+02:00 2017-08-21T14:49:08+05:30 2017-08-25T10:43:05+02:00 True iText® 5.3.5 ©2000-2012 1T3XT BVBA (AGPL-version) VoR uuid:617072a8-6d16-41ab-b2ff-aa58f5ab536d uuid:e3f9a5aa-15b2-45cd-a77c-db4ddfcddbce default 1 converted uuid:6ab23415-67bc-479c-9e41-d111d94f2ae9 converted to PDF/A-2b pdfToolbox 2017-08-21T14:49:44+05:30 2 B http://ns.adobe.com/xap/1.0/mm/ xmpMM XMP Media Management 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