e79f256a513b4d7c8a8239f073186147 molecules_a2020v25n14p3264.pdf.pdf 7d2082ccd91ad8512c6b1ecde43d84d60c4b1829 molecules_a2020v25n14p3264.pdf.pdf df95af062c5c7918e132a6d569635fad898e5e2b0b169ba126048f1aa7b2bb28 molecules_a2020v25n14p3264.pdf.pdf Title: Asymmetric Preparation of -Quaternary Fluorinated -keto Esters. Review Subject: In this review, recent advances over the past decade in the preparation of fluorinated stereogenic quaternary centers on -keto esters compounds are analyzed. Since the incorporation of fluorine and fluorinated groups is of special interest in pharmaceutical chemistry, a range of metal-catalyzed and organocatalyzed methods have been developed. Herein, we review the enantioselective fluorination, trifluoromethylation and trifluoromethylthiolation of 3-oxo esters. The scope, the induction of enantioselectivity and mechanistic investigations are presented. Keywords: fluorination; trifluoromethylation; trifluoromethylthiolation; -keto esters; asymmetric Author: Albert Granados and Adelina Vallribera Creator: LaTeX with hyperref package Producer: pdfTeX-1.40.18 CreationDate: Fri Jul 17 12:13:27 2020 CEST ModDate: Fri Jul 17 12:13:27 2020 CEST Tagged: no UserProperties: no Suspects: no Form: none JavaScript: no Pages: 24 Encrypted: no Page size: 595.276 x 841.89 pts (A4) Page rot: 0 File size: 5138305 bytes Optimized: no PDF version: 1.5 name type encoding emb sub uni object ID ------------------------------------ ----------------- ---------------- --- --- --- --------- DNFVAS+URWPalladioL-Ital Type 1 Custom yes yes no 93 0 ZAJMUN+URWPalladioL-Bold Type 1 Custom yes yes no 94 0 CWZXCD+Rpxbmi Type 1 Builtin yes yes no 95 0 DPHTFR+URWPalladioL-Roma Type 1 Custom yes yes no 96 0 CIQLLF+VnURWPalladioL Type 1 Custom yes yes no 97 0 SVVJCD+Rpxr Type 1 Builtin yes yes no 98 0 VZPSRL+Rpxmi Type 1 Builtin yes yes no 99 0 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ぁびべねねづぴひどっぜ〴ぜ〰ぐひづばちひちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰けふちぴづひのちひべぜ〴ぜ〰ぃ〭こぃう〳ぜ〴ぜ〰こぴづひづはっづのぴひづびぜ〴ぜ〰はのぜ〴ぜ〰〭にづぴはぜ〴ぜ〰ぅびぴづひびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮ㄩ‾㸊⡜㌷㙜㌷㝜〰きづぴちぬ〭ぃちぴちぬべぺづつぜ〴ぜ〰きづぴとはつびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㈩‾㸊⡜㌷㙜㌷㝜〰くひでちのはっちぴちぬべぴどっぜ〴ぜ〰きづぴとはつびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㌩‾㸊⡜㌷㙜㌷㝜〰きづぴとはつびぜ〴ぜ〰ぉのぶはぬぶどのでぜ〴ぜ〰ぃとどひちぬぜ〴ぜ〰〭こぃう〳ぜ〴ぜ〰げづちでづのぴびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸵ Children: Item: Title: きづぴちぬ〭ぃちぴちぬべぺづつぜ〴ぜ〰きづぴとはつびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㈩‾㸊⡜㌷㙜㌷㝜〰くひでちのはっちぴちぬべぴどっぜ〴ぜ〰きづぴとはつびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㌩‾㸊⡜㌷㙜㌷㝜〰きづぴとはつびぜ〴ぜ〰ぉのぶはぬぶどのでぜ〴ぜ〰ぃとどひちぬぜ〴ぜ〰〭こぃう〳ぜ〴ぜ〰げづちでづのぴびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸵ Item: Title: くひでちのはっちぴちぬべぴどっぜ〴ぜ〰きづぴとはつびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㐮㌩‾㸊⡜㌷㙜㌷㝜〰きづぴとはつびぜ〴ぜ〰ぉのぶはぬぶどのでぜ〴ぜ〰ぃとどひちぬぜ〴ぜ〰〭こぃう〳ぜ〴ぜ〰げづちでづのぴびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸵ Item: Title: きづぴとはつびぜ〴ぜ〰ぉのぶはぬぶどのでぜ〴ぜ〰ぃとどひちぬぜ〴ぜ〰〭こぃう〳ぜ〴ぜ〰げづちでづのぴびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸵ Item: Title: ぃはのっぬふびどはのびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸵ Item: Title: げづてづひづのっづび Filters: FilterPipeline: FlateDecode Fonts: Type1: Font: BaseFont: DPHTFR+URWPalladioL-Roma FontSubset: true FirstChar: 2 LastChar: 252 FontDescriptor: FontName: DPHTFR+URWPalladioL-Roma Flags: Symbolic FontBBox: -166, -283, 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Annotation: Subtype: Link Rect: 154, 123, 191, 133 Annotation: Subtype: Link Rect: 198, 123, 234, 133 Annotation: Subtype: Link Rect: 332, 96, 370, 107 Page: Sequence: 22 Annotations: Annotation: Subtype: Link Rect: 305, 702, 342, 712 Annotation: Subtype: Link Rect: 380, 663, 418, 673 Annotation: Subtype: Link Rect: 187, 638, 224, 648 Annotation: Subtype: Link Rect: 321, 611, 358, 622 Annotation: Subtype: Link Rect: 270, 585, 307, 596 Annotation: Subtype: Link Rect: 159, 560, 196, 570 Annotation: Subtype: Link Rect: 202, 560, 238, 570 Annotation: Subtype: Link Rect: 237, 534, 273, 544 Annotation: Subtype: Link Rect: 428, 495, 465, 506 Annotation: Subtype: Link Rect: 471, 495, 507, 506 Annotation: Subtype: Link Rect: 100, 457, 137, 467 Annotation: Subtype: Link Rect: 315, 430, 353, 441 Annotation: Subtype: Link Rect: 301, 404, 339, 415 Annotation: Subtype: Link Rect: 383, 353, 420, 364 Annotation: Subtype: Link Rect: 426, 353, 462, 364 Annotation: Subtype: Link Rect: 186, 315, 223, 325 Annotation: Subtype: Link Rect: 181, 263, 219, 273 Annotation: Subtype: Link Rect: 278, 237, 316, 247 Annotation: Subtype: Link Rect: 322, 237, 358, 247 Annotation: Subtype: Link Rect: 459, 198, 496, 209 Annotation: Subtype: Link Rect: 414, 172, 452, 183 Annotation: Subtype: Link Rect: 458, 172, 494, 183 Annotation: Subtype: Link Rect: 210, 146, 247, 157 Annotation: Subtype: Link Rect: 317, 120, 354, 131 Annotation: Subtype: Link Rect: 361, 120, 397, 131 Annotation: Subtype: Link Rect: 99, 82, 136, 92 Page: Sequence: 23 Annotations: Annotation: Subtype: Link Rect: 177, 715, 214, 725 Annotation: Subtype: Link Rect: 302, 688, 339, 699 Annotation: Subtype: Link Rect: 150, 651, 187, 661 Annotation: Subtype: Link Rect: 463, 624, 500, 635 Annotation: Subtype: Link Rect: 337, 598, 374, 609 Annotation: Subtype: Link Rect: 145, 560, 183, 570 Annotation: Subtype: Link Rect: 474, 533, 511, 544 Annotation: Subtype: Link Rect: 145, 496, 182, 506 Annotation: Subtype: Link Rect: 100, 457, 137, 467 Annotation: Subtype: Link Rect: 226, 418, 264, 428 Annotation: Subtype: Link Rect: 458, 391, 495, 402 Annotation: Subtype: Link Rect: 349, 366, 387, 376 Annotation: Subtype: Link Rect: 393, 366, 429, 376 Annotation: Subtype: Link Rect: 145, 328, 183, 338 Annotation: Subtype: Link Rect: 189, 328, 225, 338 Annotation: Subtype: Link Rect: 384, 301, 421, 312 Annotation: Subtype: Link Rect: 427, 301, 463, 312 Annotation: Subtype: Link Rect: 356, 275, 393, 286 Annotation: Subtype: Link Rect: 400, 275, 436, 286 Annotation: Subtype: Link Rect: 272, 237, 309, 247 Annotation: Subtype: Link Rect: 100, 199, 137, 209 Annotation: Subtype: Link Rect: 278, 172, 316, 183 Annotation: Subtype: Link Rect: 312, 146, 350, 157 Annotation: Subtype: Link Rect: 356, 146, 392, 157 Annotation: Subtype: Link Rect: 265, 107, 303, 118 Annotation: Subtype: Link Rect: 156, 82, 193, 92 Page: Sequence: 24 Annotations: Annotation: Subtype: Link Rect: 185, 689, 223, 699 Annotation: Subtype: Link Rect: 438, 663, 475, 673 Annotation: Subtype: Link Rect: 481, 663, 516, 673 Annotation: Subtype: Link Rect: 439, 637, 475, 648 Annotation: Subtype: Link Rect: 481, 637, 516, 648 Annotation: Subtype: Link Rect: 234, 612, 272, 622 Annotation: Subtype: Link Rect: 395, 572, 433, 583 Annotation: Subtype: Link Rect: 310, 546, 348, 557 Annotation: Subtype: Link Rect: 354, 546, 390, 557 Annotation: Subtype: Link Rect: 100, 508, 137, 519 Annotation: Subtype: Link Rect: 431, 443, 468, 454 Annotation: Subtype: Link Rect: 474, 443, 510, 454 Annotation: Subtype: Link Rect: 320, 418, 357, 428 Annotation: Subtype: Link Rect: 270, 391, 307, 402 Annotation: Subtype: Link Rect: 100, 354, 137, 364 Annotation: Subtype: Link Rect: 279, 314, 316, 325 Annotation: Subtype: Link Rect: 478, 275, 515, 286 Annotation: Subtype: Link Rect: 417, 249, 453, 260 Annotation: Subtype: Link Rect: 459, 249, 494, 260 Annotation: Subtype: Link Rect: 221, 212, 258, 222 Annotation: Subtype: Link Rect: 156, 173, 192, 183 Annotation: Subtype: Link Rect: 198, 173, 233, 183 Annotation: Subtype: Link Rect: 154, 134, 192, 144 Annotation: Subtype: Link Rect: 76, 92, 166, 123 Annotation: Subtype: Link Rect: 234, 86, 407, 97 Checksum: c056a41b Type: CRC32 Checksum: e79f256a513b4d7c8a8239f073186147 Type: MD5 Checksum: 7d2082ccd91ad8512c6b1ecde43d84d60c4b1829 Type: SHA-1