97ac35cc8c552298be99a2a99744fdbc pmc_31968616.pdf 69eb8227118b68d4835273b4f4eaa0ff90f8bccf pmc_31968616.pdf 96d952cf2241d45bdd1d78044b9bcee6e0de954ff4100dce8769cf51f401ed20 pmc_31968616.pdf Title: Separation and Recycling of Concentrated Heavy Metal Wastewater by Tube Membrane Distillation Integrated with Crystallization Subject: Tube membrane distillation (MD) integrated with a crystallization method is used in this study for the concurrent productions of pure water and salt crystals from concentrated single and mixed system solutions. The effects of concentrated Zn2+ and Ni2+ on performance in terms of membrane flux, permeate conductivity, crystal recovery rates, and crystal grades are investigated. Preferred crystallization and co-crystallization determinations were performed for mixed solutions. The results revealed that membrane fluxes remained at 2.61 kgm-2h-1 and showed a sharp decline until the saturation increased to 1.38. Water yield conductivity was below 10 scm-1. High concentrated zinc and nickel did not have a particular effect on the rejection of the membrane process. For the mixed solutions, membrane flux showed a sharp decrease due to the high saturation, while the conductivity of permeate remained below 10 scm-1 during the whole process. Co-crystallization has been proven to be a better method due to the existence of the SO42- common-ion effect. Membrane fouling studies have suggested that the membrane has excellent resistance to fouling from highly concentrated solutions. The MD integrated with crystallization proves to be a promising technology for treating highly concentrated heavy metal solutions. Keywords: wastewater treatment; membrane distillation; crystallization; heavy metals; concentrated solutions; membrane fouling Author: Xiang-Yang Lou, Zheng Xu, An-Ping Bai, Montserrat Resina-Gallego and Zhong-Guang Ji Creator: LaTeX with hyperref package Producer: pdfTeX-1.40.18 CreationDate: Mon Jan 20 11:14:26 2020 CET ModDate: Mon Jan 20 11:14:26 2020 CET Tagged: no UserProperties: no Suspects: no Form: none JavaScript: no Pages: 13 Encrypted: no Page size: 595.276 x 841.89 pts (A4) Page rot: 0 File size: 4078983 bytes Optimized: no PDF version: 1.5 name type encoding emb sub uni object ID ------------------------------------ ----------------- ---------------- --- --- --- --------- RYRBZH+URWPalladioL-Ital Type 1 Custom yes yes no 82 0 RACFZO+URWPalladioL-Bold Type 1 Custom yes yes no 83 0 YOIWZZ+URWPalladioL-Roma Type 1 Custom yes yes no 84 0 HAPMKG+VnURWPalladioL Type 1 Custom yes yes no 85 0 MHAHCD+Rpxr Type 1 Builtin yes yes no 86 0 PCLMRN+Pxsy Type 1 Builtin yes yes no 87 0 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650 0 Jhove (Rel. 1.22.1, 2019-04-17) Date: 2020-11-18 07:06:01 CET RepresentationInformation: pmc_31968616.pdf ReportingModule: PDF-hul, Rel. 1.12.1 (2019-04-17) LastModified: 2020-03-16 03:55:26 CET Size: 4078983 Format: PDF Version: 1.5 Status: Well-Formed and valid SignatureMatches: PDF-hul MIMEtype: application/pdf PDFMetadata: Objects: 0 FreeObjects: 2 IncrementalUpdates: 0 DocumentCatalog: ViewerPreferences: HideToolbar: false HideMenubar: false HideWindowUI: false FitWindow: true CenterWindow: false DisplayDocTitle: false NonFullScreenPageMode: UseNone Direction: L2R ViewArea: CropBox ViewClip: CropBox PrintArea: CropBox PageClip: CropBox PageLayout: SinglePage PageMode: UseNone Outlines: Item: Title: ぉのぴひはつふっぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸲ Item: Title: きちぴづひどちぬびぜ〴ぜ〰ちのつぜ〴ぜ〰きづぴとはつびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮ㄩ‾㸊⡜㌷㙜㌷㝜〰きちぴづひどちぬびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㈩‾㸊⡜㌷㙜㌷㝜〰きづねぢひちのづぜ〴ぜ〰ぃとちひちっぴづひどぺちぴどはのびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㌩‾㸊⡜㌷㙜㌷㝜〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰ぅへばづひどねづのぴびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㐩‾㸊⡜㌷㙜㌷㝜〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰ぃとちひちっぴづひどぺちぴどはのびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸳ Children: Item: Title: きちぴづひどちぬびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㈩‾㸊⡜㌷㙜㌷㝜〰きづねぢひちのづぜ〴ぜ〰ぃとちひちっぴづひどぺちぴどはのびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㌩‾㸊⡜㌷㙜㌷㝜〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰ぅへばづひどねづのぴびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㐩‾㸊⡜㌷㙜㌷㝜〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰ぃとちひちっぴづひどぺちぴどはのびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸳ Item: Title: きづねぢひちのづぜ〴ぜ〰ぃとちひちっぴづひどぺちぴどはのびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㌩‾㸊⡜㌷㙜㌷㝜〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰ぅへばづひどねづのぴびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㐩‾㸊⡜㌷㙜㌷㝜〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰ぃとちひちっぴづひどぺちぴどはのびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸳ Item: Title: きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰ぅへばづひどねづのぴびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㈮㐩‾㸊⡜㌷㙜㌷㝜〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰ぃとちひちっぴづひどぺちぴどはのびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸳ Item: Title: きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰ぃとちひちっぴづひどぺちぴどはのびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸳ Item: Title: げづびふぬぴびぜ〴ぜ〰ちのつぜ〴ぜ〰いどびっふびびどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮ㄩ‾㸊⡜㌷㙜㌷㝜〰こどのでぬづぜ〴ぜ〰こべびぴづねぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㈩‾㸊⡜㌷㙜㌷㝜〰ぐひづてづひづのぴどちぬぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ずどのっぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㌩‾㸊⡜㌷㙜㌷㝜〰ぐひづてづひづのぴどちぬぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぎどっにづぬぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㐩‾㸊⡜㌷㙜㌷㝜〰ぃは〭ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ずどのっぜ〴ぜ〰ちのつぜ〴ぜ〰ぎどっにづぬぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㔩‾㸊⡜㌷㙜㌷㝜〰きづねぢひちのづぜ〴ぜ〰うはふぬどのでぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Children: Item: Title: こどのでぬづぜ〴ぜ〰こべびぴづねぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㈩‾㸊⡜㌷㙜㌷㝜〰ぐひづてづひづのぴどちぬぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ずどのっぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㌩‾㸊⡜㌷㙜㌷㝜〰ぐひづてづひづのぴどちぬぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぎどっにづぬぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㐩‾㸊⡜㌷㙜㌷㝜〰ぃは〭ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ずどのっぜ〴ぜ〰ちのつぜ〴ぜ〰ぎどっにづぬぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㔩‾㸊⡜㌷㙜㌷㝜〰きづねぢひちのづぜ〴ぜ〰うはふぬどのでぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Item: Title: ぐひづてづひづのぴどちぬぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ずどのっぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㌩‾㸊⡜㌷㙜㌷㝜〰ぐひづてづひづのぴどちぬぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぎどっにづぬぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㐩‾㸊⡜㌷㙜㌷㝜〰ぃは〭ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ずどのっぜ〴ぜ〰ちのつぜ〴ぜ〰ぎどっにづぬぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㔩‾㸊⡜㌷㙜㌷㝜〰きづねぢひちのづぜ〴ぜ〰うはふぬどのでぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Item: Title: ぐひづてづひづのぴどちぬぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ぎどっにづぬぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㐩‾㸊⡜㌷㙜㌷㝜〰ぃは〭ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ずどのっぜ〴ぜ〰ちのつぜ〴ぜ〰ぎどっにづぬぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㔩‾㸊⡜㌷㙜㌷㝜〰きづねぢひちのづぜ〴ぜ〰うはふぬどのでぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Item: Title: ぃは〭ぃひべびぴちぬぬどぺちぴどはのぜ〴ぜ〰はてぜ〴ぜ〰ずどのっぜ〴ぜ〰ちのつぜ〴ぜ〰ぎどっにづぬぜ〴ぜ〰こふぬてちぴづぜ〴ぜ〰ぢべぜ〴ぜ〰きいぜ〴ぜ〰ぉのぴづでひちぴづつぜ〴ぜ〰ぷどぴとぜ〴ぜ〰ぃひべびぴちぬぬどぺちぴどはのぜ〴〩਼㰠⽓ 䝯呯 䐠⡳畢獥捴楯渮㌮㔩‾㸊⡜㌷㙜㌷㝜〰きづねぢひちのづぜ〴ぜ〰うはふぬどのでぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Item: Title: きづねぢひちのづぜ〴ぜ〰うはふぬどのでぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Item: Title: ぃはのっぬふびどはのびぜ〴〩਼㰠⽓ 䝯呯 䐠⡳散瑩潮⸴ Item: Title: げづてづひづのっづび Filters: FilterPipeline: FlateDecode Fonts: Type1: Font: BaseFont: RYRBZH+URWPalladioL-Ital FontSubset: true FirstChar: 45 LastChar: 122 FontDescriptor: FontName: RYRBZH+URWPalladioL-Ital Flags: Symbolic FontBBox: -170, -305, 1010, 941 FontFile: true EncodingDictionary: Differences: true Font: BaseFont: RACFZO+URWPalladioL-Bold FontSubset: true FirstChar: 3 LastChar: 122 FontDescriptor: FontName: RACFZO+URWPalladioL-Bold Flags: Symbolic FontBBox: -152, -301, 1000, 935 FontFile: true EncodingDictionary: Differences: true Font: BaseFont: YOIWZZ+URWPalladioL-Roma FontSubset: true FirstChar: 2 LastChar: 241 FontDescriptor: FontName: YOIWZZ+URWPalladioL-Roma Flags: Symbolic FontBBox: -166, -283, 1021, 943 FontFile: true EncodingDictionary: Differences: true Font: BaseFont: HAPMKG+VnURWPalladioL FontSubset: true FirstChar: 162 LastChar: 225 FontDescriptor: FontName: HAPMKG+VnURWPalladioL 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