95759b10626bf7e2597f4f345c598366 pmc_33801138.pdf 2d14788326b3591e18dce5732934ea9abf183cea pmc_33801138.pdf 64f0a737e2b8aabf0b2f81abc57c376a66d7466126c27c4583c70c3b89cc25b1 pmc_33801138.pdf Title: Recycled Mortars with Ceramic Aggregates. Pore Network Transmutation and Its Relationship with Physical and Mechanical Properties Subject: The porosity of mortars with recycled ceramic aggregates (10, 20, 30, 50, and 100% as a replacement of natural aggregate) was evaluated and analyzed using three different techniques. The results of gas adsorption (N2), Scanning Electron Microscopy (SEM) image analysis and open porosity allowed establishing the relationship between the recycled aggregate content and the porosity of these mortars, as well as the relationship between porosity and the physical and mechanical properties of the mortars: absorption, density, compressive strength, modulus of elasticity, and drying shrinkage. Using the R2 coefficient and the equation typology as criteria, additional data such as Brunauer, Emmett, and Teller (BET) surface area (N2 adsorption) established significant correlations with the mentioned properties; with SEM image analysis, no explanatory relationships could be established; and with open porosity, revealing relationships were established (R2 > 0.9). With the three techniques, it was confirmed that the increase in porosity is related to the increase in the amount of ceramic aggregate; in particular with gas adsorption (N2) and open porosity. It was concluded that the open porosity technique can explain the behavior of these recycled mortars with more reliable data, in a simple and direct way, linked to its establishment with a more representative sample of the mortar matrix. Keywords: recycled mortars; ceramic wastes; recycled aggregates; porosity; adsorption N2; image analysis; open porosity Author: Francisca Guadalupe Cabrera-Covarrubias, José Manuel Gómez-Soberón, Carlos Antonio Rosas-Casarez, Jorge Luis Almaral-Sánchez and Jesús Manuel Bernal-Camacho Creator: LaTeX with hyperref Producer: pdfTeX-1.40.21 CreationDate: Tue Mar 23 06:55:34 2021 CET ModDate: Tue Mar 23 07:02:43 2021 CET Custom Metadata: no Metadata Stream: no Tagged: no UserProperties: no Suspects: no Form: none JavaScript: no Pages: 23 Encrypted: no Page size: 595.276 x 841.89 pts (A4) Page rot: 0 File size: 9571385 bytes Optimized: no PDF version: 1.7 name type encoding emb sub uni object ID ------------------------------------ ----------------- ---------------- --- --- --- --------- WQSWES+URWPalladioL-Ital Type 1 Custom yes yes no 10 0 YKSFIK+URWPalladioL-Bold Type 1 Custom yes yes no 15 0 TYFZSO+URWPalladioL-Roma Type 1 Custom yes yes no 19 0 DGBDNV+VnURWPalladioL-Bold Type 1 Custom 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ABCDEE+Palatino Linotype TrueType WinAnsi yes yes no 654 0 ABCDEE+Palatino Linotype,Italic TrueType WinAnsi yes yes no 658 0 ABCDEE+Palatino Linotype CID TrueType Identity-H yes yes yes 662 0 SYVAVM+VnURWPalladioL-Italic Type 1 Custom yes yes no 681 0 Jhove (Rel. 1.28.0, 2023-05-18) Date: 2024-10-02 03:25:35 CEST RepresentationInformation: pmc_33801138.pdf ReportingModule: PDF-hul, Rel. 1.12.4 (2023-03-16) LastModified: 2023-03-31 12:09:24 CEST Size: 9571385 Format: PDF Version: 1.7 Status: Well-Formed and valid SignatureMatches: PDF-hul MIMEtype: application/pdf PDFMetadata: Objects: 887 FreeObjects: 1 IncrementalUpdates: 0 DocumentCatalog: PageLayout: SinglePage PageMode: UseNone Outlines: Item: Title: Introduction Destination: section.1 Item: Title: Materials and Methods Destination: section.2 Children: Item: Title: Materials Destination: subsection.2.1 Item: Title: Properties of Study Aggregates Destination: subsection.2.2 Item: Title: Mortar Mixes Destination: subsection.2.3 Item: Title: Physical and Mechanical Properties Tests Destination: subsection.2.4 Item: Title: Nitrogen (N2) Adsorption Porosimetry Destination: subsection.2.5 Item: Title: Porosity by SEM and Microanalysis of Chemical Elements with an Energy Dispersive Spectrometer (SEM-EDS) Destination: subsection.2.6 Item: Title: Image Analysis (Obtained with Scanning Electron Microscope SEM), Using NI Vision Assistant Destination: subsection.2.7 Item: Title: Results and Discussion Destination: section.3 Children: Item: Title: Physical and Mechanical Properties of CRMs Destination: subsection.3.1 Item: Title: Porosimetry by N2 Adsorption Destination: subsection.3.2 Item: Title: Porosimetry by SEM Image Analysis Destination: subsection.3.3 Item: Title: Total Open Porosity Destination: subsection.3.4 Item: Title: Correlations between Porosimetry Techniques Destination: subsection.3.5 Item: Title: Conclusions Destination: section.4 Item: Title: References Destination: Item.8 Info: Title: Recycled Mortars with Ceramic Aggregates. Pore Network Transmutation and Its Relationship with Physical and Mechanical Properties Author: Francisca Guadalupe Cabrera-Covarrubias, José Manuel Gómez-Soberón, Carlos Antonio Rosas-Casarez, Jorge Luis Almaral-Sánchez and Jesús Manuel Bernal-Camacho Subject: The porosity of mortars with recycled ceramic aggregates (10, 20, 30, 50, and 100% as a replacement of natural aggregate) was evaluated and analyzed using three different techniques. The results of gas adsorption (N2), Scanning Electron Microscopy (SEM) image analysis and open porosity allowed establishing the relationship between the recycled aggregate content and the porosity of these mortars, as well as the relationship between porosity and the physical and mechanical properties of the mortars: absorption, density, compressive strength, modulus of elasticity, and drying shrinkage. Using the R2 coefficient and the equation typology as criteria, additional data such as Brunauer, Emmett, and Teller (BET) surface area (N2 adsorption) established significant correlations with the mentioned properties; with SEM image analysis, no explanatory relationships could be established; and with open porosity, revealing relationships were established (R2 > 0.9). With the three techniques, it was confirmed that the increase in porosity is related to the increase in the amount of ceramic aggregate; in particular with gas adsorption (N2) and open porosity. It was concluded that the open porosity technique can explain the behavior of these recycled mortars with more reliable data, in a simple and direct way, linked to its establishment with a more representative sample of the mortar matrix. 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