41fe1946f0774db9dd4ca2ca661979ae Davtian_jcA_2023.pdf 724a576ba03dc7a143c364c91914b5a5934a20e2 Davtian_jcA_2023.pdf 37f337af513b2457ba7e882f121c4ab44045bfa313b43f6ad7935d713fe2ab75 Davtian_jcA_2023.pdf Title: Selective extraction of levoglucosan and its isomers from complex matrices using ligand exchange-solid phase extraction for analysis by liquid chromatography-electrospray ionization-tandem mass spectrometry Subject: Journal of Chromatography A, 1695 (2023) 463935. doi:10.1016/j.chroma.2023.463935 Keywords: "Biomass burning"; "Levoglucosan"; "Sediment samples"; "Liquid chromatography-electrospray ionization-tandem mass spectrometry"; "Ligand exchange-solid phase extraction" Author: Nina Davtian Creator: Elsevier Producer: Acrobat Distiller 10.0.0 (Windows) CreationDate: Thu Mar 23 20:42:32 2023 CET ModDate: Thu Mar 23 20:43:13 2023 CET Tagged: yes UserProperties: no Suspects: no Form: none JavaScript: no Pages: 10 Encrypted: no Page size: 595.245 x 793.92 pts Page rot: 0 File size: 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UseOutlines Language: English Outlines: Item: Title: Selective extraction of levoglucosan and its isomers from complex matrices using ligand exchange-solid phase extraction for analysis by liquid chromatography-electrospray ionization-tandem mass spectrometry Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@6a1aab78 Children: Item: Title: 1 Introduction Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@462d5aee Item: Title: 2 Materials and methods Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@69b0fd6f Children: Item: Title: 2.1 Standards, solvents, and reagents Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@757942a1 Item: Title: 2.2 Sediment samples Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@4a87761d Item: Title: 2.3 Extraction method Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@66d1af89 Item: Title: 2.4 LE-SPE purification method Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@8646db9 Item: Title: 2.5 Extract desalting and concentration Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@37374a5e Item: Title: 2.6 LC-MS/MS analysis Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@4671e53b Item: Title: 2.7 Quantification of MAs and estimation of ion suppression Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@2db7a79b Item: Title: 2.8 Method validation Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@6950e31 Item: Title: 3 Results Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@b7dd107 Children: Item: Title: 3.1 LC-MS/MS detection setup Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@42eca56e Item: Title: 3.2 Ligand exchange-solid phase extraction (LE-SPE) Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@52f759d7 Item: Title: 3.3 Optimization of the selective pressurized liquid extraction Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@7cbd213e Item: Title: 3.4 Extract desalting Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@192d3247 Item: Title: 3.5 Method validation Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@3ecd23d9 Children: Item: Title: 3.5.1 Linearity and sensitivity Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@569cfc36 Item: Title: 3.5.2 Repeatability Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@43bd930a Item: Title: 3.5.3 Blank contributions Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@33723e30 Item: Title: 3.5.4 Total and mass IS recovery and ion suppression effect Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@64f6106c Item: Title: 4 Discussion Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@553a3d88 Item: Title: 5 Conclusions Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@7a30d1e6 Item: Title: Declaration of competing interest Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@5891e32e Item: Title: CRediT authorship contribution statement Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@cb0ed20 Item: Title: Funding Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@8e24743 Item: Title: Acknowledgements Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@74a10858 Item: Title: Supplementary materials Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@23fe1d71 Item: Title: References Destination: edu.harvard.hul.ois.jhove.module.pdf.PdfSimpleObject@28ac3dc3 Info: Title: Selective extraction of levoglucosan and its isomers from complex matrices using ligand exchange-solid phase extraction for analysis by liquid chromatography-electrospray ionization-tandem mass spectrometry Author: Nina Davtian Subject: Journal of Chromatography A, 1695 (2023) 463935. doi:10.1016/j.chroma.2023.463935 Keywords: "Biomass burning"; "Levoglucosan"; "Sediment samples"; "Liquid chromatography-electrospray ionization-tandem mass spectrometry"; "Ligand exchange-solid phase extraction" Creator: Elsevier Producer: Acrobat Distiller 10.0.0 (Windows) CreationDate: Thu Mar 23 21:12:32 CET 2023 ModDate: Thu Mar 23 21:13:13 CET 2023 ID: 0x37b191c58f6475f4c7c3e35e4a1ab1a6, 0xae29750486eacd83e217bc4406e6dfa1 Filters: FilterPipeline: FlateDecode FilterPipeline: DCTDecode Images: Image: NisoImageMetadata: FormatName: image/jpg CompressionScheme: JPEG ImageWidth: 249 ImageHeight: 273 ColorSpace: RGB BitsPerSample: 8 BitsPerSampleUnit: integer Image: NisoImageMetadata: FormatName: image/png ImageWidth: 118 ImageHeight: 118 BitsPerSample: 8 BitsPerSampleUnit: integer Filter: FlateDecode Image: NisoImageMetadata: FormatName: image/jpg CompressionScheme: JPEG ImageWidth: 223 ImageHeight: 297 ColorSpace: RGB BitsPerSample: 8 BitsPerSampleUnit: integer Image: NisoImageMetadata: FormatName: image/jpg 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Journal of Chromatography A, 1695 (2023) 463935. doi:10.1016/j.chroma.2023.463935 Biomass burning Levoglucosan Sediment samples Liquid chromatography-electrospray ionization-tandem mass spectrometry Ligand exchange-solid phase extraction Selective extraction of levoglucosan and its isomers from complex matrices using ligand exchange-solid phase extraction for analysis by liquid chromatography-electrospray ionization-tandem mass spectrometry Nina Davtian Nuria Penalva Antoni Rosell-Melé Joan Villanueva uuid:fd8cfc10-4791-4a8b-8025-00abb91efa0c uuid:060033fa-dea1-47ab-aa75-2e9a85f0b63f journal © 2023 The Author(s). Published by Elsevier B.V. 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Subtype: Link Rect: 320, 121, 579, 141 Annotation: Subtype: Link Rect: 320, 81, 579, 101 Annotation: Subtype: Link Rect: 382, 50, 438, 58 Page: Label: 10 Annotations: Annotation: Subtype: Link Rect: 114, 688, 190, 695 Annotation: Subtype: Link Rect: 25, 647, 294, 667 Annotation: Subtype: Link Rect: 25, 607, 294, 627 Annotation: Subtype: Link Rect: 178, 569, 268, 576 Annotation: Subtype: Link Rect: 167, 537, 238, 544 Annotation: Subtype: Link Rect: 25, 496, 294, 516 Annotation: Subtype: Link Rect: 385, 696, 457, 703 Annotation: Subtype: Link Rect: 442, 672, 541, 679 Annotation: Subtype: Link Rect: 356, 640, 427, 647 Annotation: Subtype: Link Rect: 332, 616, 426, 623 Annotation: Subtype: Link Rect: 320, 583, 579, 603 Annotation: Subtype: Link Rect: 346, 553, 432, 560 Annotation: Subtype: Link Rect: 475, 497, 551, 504 Checksum: 2111725f Type: CRC32 Checksum: 41fe1946f0774db9dd4ca2ca661979ae Type: MD5 Checksum: 724a576ba03dc7a143c364c91914b5a5934a20e2 Type: SHA-1