811d1ce894d1408e711aa56df3a373cd pmc_10338372.pdf 99646bb3aaa1cbc172517c770a9070e8c926a6d7 pmc_10338372.pdf 940d4e074a60dfff87a6aa7ab6a343f2719e6a5c6f86937061c5a80ae6c0b4f2 pmc_10338372.pdf Title: Synthesis and characterization of highly diluted polyanionic iron(II) spin crossover systems Subject: STAR Protocols, 4 (2023) 102394. doi:10.1016/j.xpro.2023.102394 Author: Andrea Moneo-Corcuera Creator: Elsevier Producer: Acrobat Distiller 8.1.0 (Windows) CreationDate: Fri Jun 30 03:17:51 2023 CEST ModDate: Fri Jun 30 03:18:38 2023 CEST Custom Metadata: yes Metadata Stream: yes Tagged: no UserProperties: no Suspects: no Form: none JavaScript: no Pages: 22 Encrypted: no Page size: 602.986 x 782.986 pts Page rot: 0 File size: 7444247 bytes Optimized: yes PDF version: 1.7 name type encoding emb sub uni object ID ------------------------------------ ----------------- ---------------- --- --- --- --------- BDLLBH+AdvPSA5BC Type 1C WinAnsi yes yes no 854 0 BDLLBI+AdvPSA5CD Type 1C WinAnsi yes yes 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characterization of highly diluted polyanionic iron(II) spin crossover systems Destination: titlink1 Children: Item: Title: Before you begin Destination: flink1 Item: Title: Key resources table Destination: flink2 Item: Title: Step-by-step method details Destination: flink3 Children: Item: Title: Synthesis of the triazol-based ligand (Me2NH2)2L) Destination: slink1 Item: Title: Synthesis of FeII and ZnII coordination complexes Destination: slink2 Item: Title: Structure of FeII and ZnII coordination complexes Destination: slink3 Children: Item: Title: Single-crystal X-Ray diffraction (SCXRD) Destination: tlink1 Item: Title: Powder X-ray diffraction (PXRD) Destination: tlink2 Item: Title: Spin transition detection of the iron trimer (Fe3) in Zn3(1-x)Fe3x Destination: slink4 Children: Item: Title: Magnetic measurements Destination: tlink3 Item: Title: Spin transition detection of the polyanionic trimers in the liquid state Destination: slink5 Item: Title: Expected outcomes Destination: flink4 Item: Title: Limitations Destination: flink5 Item: Title: Troubleshooting Destination: flink6 Children: Item: Title: Problem 1 Destination: slink6 Item: Title: Potential solution Destination: slink7 Item: Title: Problem 2 Destination: slink8 Item: Title: Potential solution Destination: slink9 Item: Title: Problem 3 Destination: slink10 Item: Title: Potential solution Destination: slink11 Item: Title: Problem 4 Destination: slink12 Item: Title: Potential solution Destination: slink13 Item: Title: Problem 5 Destination: slink14 Item: Title: Potential solution Destination: slink15 Item: Title: Resource availability Destination: flink7 Children: Item: Title: Lead contact Destination: slink16 Item: Title: Materials availability Destination: slink17 Item: Title: Data and code availability Destination: slink18 Item: Title: Acknowledgments Destination: acklink1 Item: Title: Author contributions Destination: flink8 Item: Title: Declaration of interests Destination: flink9 Item: Title: 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Nieto-Castro Jordi Cirera Verónica Gómez Jesús Sanjosé-Orduna Carla Casadevall Gábor Molnár Azzedine Bousseksou Teodor Parella José María Martínez-Agudo Julio Lloret-Fillol Mónica Helvia Pérez-Temprano Eliseo Ruiz José Ramón Galán-Mascarós Molecular/Chemical Probes Chemistry Material Sciences STAR Protocols, 4 (2023) 102394. doi:10.1016/j.xpro.2023.102394 The Authors journal STAR Protocols © 2023 The Authors. 2666-1667 4 3 15 September 2023 2023-09-15 102394 102394 10.1016/j.xpro.2023.102394 https://doi.org/10.1016/j.xpro.2023.102394 2010-04-23 true 10.1016/j.xpro.2023.102394 elsevier.com sciencedirect.com VoR 7.0 10.1016/j.xpro.2023.102394 noindex true 2010-04-23 true sciencedirect.com elsevier.com Elsevier 2023-06-30T06:47:51+05:30 2023-06-30T06:48:38+05:30 2023-06-30T06:48:38+05:30 True Acrobat Distiller 8.1.0 (Windows) uuid:487e47e5-e037-4ff8-8eb3-c1ff7a12360e uuid:a1e9417b-27eb-4844-87c2-1318f8c43286 http://creativecommons.org/licenses/by-nc-nd/4.0/ Pages: Page: Label: 1 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