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29 p, 1.1 MB Enzymatic Synthesis of Trimethyl-ϵ-caprolactone : Process Intensification and Demonstration on a 100 L Scale / Solé Ferré, Jordi (Universitat Autònoma de Barcelona. Departament d'Enginyeria Química, Biològica i Ambiental) ; Brummund, Jan (InnoSyn B.V.) ; Caminal i Saperas, Glòria (Institut de Química Avançada de Catalunya) ; Álvaro, Gregorio (Universitat Autònoma de Barcelona. Departament d'Enginyeria Química, Biològica i Ambiental) ; Schürmann, Martin (InnoSyn B.V.) ; Guillén, Marina (Universitat Autònoma de Barcelona. Departament d'Enginyeria Química, Biològica i Ambiental)
Optimization and scaling up of the Baeyer-Villiger oxidation of 3,3,5-trimethyl-cyclohexanone to trimethyl-ε-caprolactones (CHLs) were studied to demonstrate this technology on a 100 L pilot plant scale. [...]
2019 - 10.1021/acs.oprd.9b00185
Organic process research and development, Vol. 23, Issue 11 (November 2019) , p. 2336-2344  
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