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9 p, 2.1 MB Scalable Heating-Up Synthesis of Monodisperse Cu2ZnSnS4 Nanocrystals / Shavel, Alexey (Institut de Recerca en Energia de Catalunya) ; Ibáñez, Maria (Institut de Recerca en Energia de Catalunya) ; Luo, Zhishan (Institut de Recerca en Energia de Catalunya) ; De Roo, Jonathan (Ghent University. Department of Inorganic and Physical Chemistry) ; Carrete, Alex (Institut de Recerca en Energia de Catalunya) ; Dimitrievska, Mirjana (Institut de Recerca en Energia de Catalunya) ; Genç, Aziz (Institut Català de Nanociència i Nanotecnologia) ; Meyns, Michaela (Institut de Recerca en Energia de Catalunya) ; Pérez-Rodríguez, Alejandro (Institut de Recerca en Energia de Catalunya) ; Kovalenko, Maksym V. (Institute of Inorganic Chemistry (Bratislava, Eslovàquia)) ; Arbiol i Cobos, Jordi (Institut Català de Nanociència i Nanotecnologia) ; Cabot, Andreu (Institut de Recerca en Energia de Catalunya)
Monodisperse CuZnSnS (CZTS) nanocrystals (NCs), with quasi-spherical shape, were prepared by a facile, high-yield, scalable, and high-concentration heat-up procedure. The key parameters to minimize the NC size distribution were efficient mixing and heat transfer in the reaction mixture through intensive argon bubbling and improved control of the heating ramp stability. [...]
2016 - 10.1021/acs.chemmater.5b03417
Chemistry of Materials, Vol. 28, Núm. 3 (February 2016) , p. 720-726  

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