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10 p, 646.8 KB |
Synthesis of polycarboxylate rhodium(II) metal-organic polyhedra (MOPs) and their use as building blocks for highly connected metal-organic frameworks (MOFs)
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Grancha, Thais (Institut Català de Nanociència i Nanotecnologia) ;
Carné-Sánchez, Arnau (Institut Català de Nanociència i Nanotecnologia) ;
Zarekarizi, Farnoosh (Tarbiat Modares University. Department of Chemistry) ;
Hernández López, Laura (Institut Català de Nanociència i Nanotecnologia) ;
Albalad, Jorge (Institut Català de Nanociència i Nanotecnologia) ;
Khobotov Bakishev, Akim (Institut Català de Nanociència i Nanotecnologia) ;
Guillerm, Vincent (Institut Català de Nanociència i Nanotecnologia) ;
Morsali, Ali (Tarbiat Modares University. Department of Chemistry) ;
Juanhuix, Judith (ALBA Laboratori de Llum de Sincrotró) ;
Gándara, Felipe (Instituto de Ciencia de Materiales de Madrid) ;
Imaz, Inhar (Institut Català de Nanociència i Nanotecnologia) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia)
Use of preformed metal-organic polyhedra (MOPs) as supermolecular building blocks (SBBs) for the synthesis of metal-organic frameworks (MOFs) remains underexplored due to lack of robust functionalized MOPs. [...]
2021 -  10.1002/anie.202013839
Angewandte Chemie (International ed. Internet), Vol. 60, issue 11 (March 2021) , p. 5729-5733
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2.
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11 p, 12.4 MB |
Solvent-tuned ultrasonic synthesis of 2D coordination polymer nanostructures and flakes
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Pepió, Belén (Institut Català de Nanociència i Nanotecnologia) ;
Contreras Pereda, Noemí (Institut Català de Nanociència i Nanotecnologia) ;
Suárez García, Salvio (Institut Català de Nanociència i Nanotecnologia) ;
Hayati, Payam (Institut Català de Nanociència i Nanotecnologia) ;
Benmansour Souilamas, Samia (Universitat de València. Institut de Ciència Molecular) ;
Retailleau, Pascal (Centre national de la recherche scientifique (França). Institut de Chimie des Substances Naturelles) ;
Morsali, Ali (Tarbiat Modares University. Faculty of Sciences) ;
Ruiz-Molina, Daniel (Institut Català de Nanociència i Nanotecnologia)
Herein, a new 2-dimensional coordination polymer based on copper (II), {Cu₂(L)(DMF₂)}n, where L stands for 1,2,4,5-benzenetetracarboxylate (complex 1) is synthesized. Interestingly, we demonstrate that both solvent and sonication are relevant in the top-down fabrication of nanostructures. [...]
2021 - 10.1016/j.ultsonch.2020.105425
Ultrasonics sonochemistry, Vol. 72 (April 2021) , art. 105425
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3.
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8 p, 1.0 MB |
Net-clipping : an approach to deduce the topology of metal-organic frameworks built with zigzag ligands
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Ortín-Rubio, Borja (Institut Català de Nanociència i Nanotecnologia) ;
Ghasempour, Hosein (Tarbiat Modares University. Department of Chemistry) ;
Guillerm, Vincent (Institut Català de Nanociència i Nanotecnologia) ;
Morsali, Ali (Tarbiat Modares University. Department of Chemistry) ;
Juanhuix, Judith (ALBA Laboratori de Llum de Sincrotró) ;
Imaz, Inhar (Institut Català de Nanociència i Nanotecnologia) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia)
Herein we propose a new approach for deducing the topology of metal-organic frameworks (MOFs) assembled from organic ligands of low symmetry, which we call net-clipping. It is based on the construction of nets by rational deconstruction of edge-transitive nets comprising higher-connected molecular building blocks (MBBs). [...]
2020 - 10.1021/jacs.0c03404
Journal of the American Chemical Society, Vol. 142, issue 20 (May 2020) , p. 9135-9140
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6 p, 1.1 MB |
Selective CO₂ capture in metal-organic frameworks with azine-functionalized pores generated by mechanosynthesis
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Masoomi, Mohammad Yaser (Tarbiat Modares University. Department of Chemistry) ;
Stylianou, Kyriakos C. (Institut Català de Nanociència i Nanotecnologia) ;
Morsali, Ali (Tarbiat Modares University. Department of Chemistry) ;
Retailleau, Pascal (Centre national de la recherche scientifique (França). Institut de Chimie des Substances Naturelles) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia)
Two new three-dimensional porous Zn(II)-based metal-organic frameworks, containing azine-functionalized pores, have been readily and quickly isolated via mechanosynthesis, by using a nonlinear dicarboxylate and linear N-donor ligands. [...]
2014 - 10.1021/cg500033b
Crystal Growth and Design, Vol. 14, issue 5 (May 2014) , p. 2092-2096
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38 p, 1.5 MB |
Sonochemical synthesis, characterization, and effects of temperature, power ultrasound and reaction time on the morphological properties of two new nanostructured mercury(II) coordination supramolecule compounds
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Hayati, Payam (University of Sistan and Baluchestan. Department of Chemistry) ;
Rezvani, Ali Reza (University of Sistan and Baluchestan. Department of Chemistry) ;
Morsali, Ali (Tarbiat Modares University. Department of Chemistry) ;
Ruiz-Molina, Daniel (Institut Català de Nanociència i Nanotecnologia) ;
Geravand, Samira (University of Sistan and Baluchestan. Department of Chemistry) ;
Suárez García, Salvio (Institut Català de Nanociència i Nanotecnologia) ;
Moreno Villaécija, Miguel Ángel (Institut Català de Nanociència i Nanotecnologia) ;
García Granda, S. (Universidad de Oviedo. Departamento de Química Física y Analítica) ;
Mendoza Meroño, Rafael (Universidad de Oviedo. Departamento de Química Física y Analítica) ;
Retailleau, Pascal (Université Paris-Saclay)
Two new mercury(II) coordination supramolecular compounds (CSCs) (1D and 0D), [Hg(L)(I)] (1) and [Hg(L')(SCN)]·2HO (2) (L = 2-amino-4-methylpyridine and L' = 2,6-pyridinedicarboxlic acid), have been synthesized under different experimental conditions. [...]
2017 - 10.1016/j.ultsonch.2017.01.021
Ultrasonics sonochemistry, Vol. 37 (July 2017) , p. 382-393
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6.
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22 p, 514.6 KB |
Sonochemical synthesis and characterization of a novel hetro-binuclear metal organic nano polymer based on picolinic acid ligand
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Hayati, Payam (Institut Català de Nanociència i Nanotecnologia) ;
Souri, Bagher (University of Sistan and Baluchestan. Department of Chemistry) ;
Rezvani, Ali Reza (University of Sistan and Baluchestan. Department of Chemistry) ;
Morsali, Ali (Tarbiat Modares University. Department of Chemistry) ;
Gutiérrez Alonso, Ángel (Universidad Complutense de Madrid. Departamento de Química Inorgánica)
Nanoparticles of one new lead and K coordination polymer (CP), {[Pb(pyc)(N)K]. ½HO} (1) Hpyc = picolinic acid ligand, has been synthesized by use of a sonochemical process and characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRPD), Fourier transform infrared spectroscopy (FTIR) spectroscopy and elemental analyses. [...]
2017 - 10.1016/j.molstruc.2017.09.006
Journal of molecular structure, Vol. 1150 (December 2017) , p. 404-410
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7.
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36 p, 2.9 MB |
Sonochemical synthesis of two novel Pb(II) 2D metal coordination polymer complexes : new precursor for facile fabrication of lead(II) oxide/bromide micro-nanostructures
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Hayati, Payam (Institut Català de Nanociència i Nanotecnologia) ;
Suárez García, Salvio (Institut Català de Nanociència i Nanotecnologia) ;
Gutiérrez Alonso, Ángel (Universidad Complutense de Madrid. Departamento de Química Inorgánica) ;
Şahin, Ertan (Ataturk University. Department of Chemistry) ;
Ruiz-Molina, Daniel (Institut Català de Nanociència i Nanotecnologia) ;
Morsali, Ali (Tarbiat Modares University. Department of Chemistry) ;
Rezvani, Ali Reza (University of Sistan and Baluchestan. Department of Chemistry)
Two new lead(II) coordination polymer complexes (CSCs) (2D), [Pb(L)(Br)]·HO (1), [Pb(HL)(L)(HO)]·HO (2), where L = CHNO (2-pyridinecarboxylic acid) and L = CHO (1,3,5-tricarboxylic acid), have been synthesized under different experimental conditions. [...]
2018 - 10.1016/j.ultsonch.2017.11.037
Ultrasonics sonochemistry, Vol. 42 (April 2018) , p. 310-319
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32 p, 2.0 MB |
Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters
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Hayati, Payam (Institut Català de Nanociència i Nanotecnologia) ;
Suárez García, Salvio (Institut Català de Nanociència i Nanotecnologia) ;
Gutiérrez Alonso, Ángel (Universidad Complutense de Madrid. Departamento de Química Inorgánica) ;
Ruiz-Molina, Daniel (Institut Català de Nanociència i Nanotecnologia) ;
Morsali, Ali (Tarbiat Modares University. Department of Chemistry) ;
Rezvani, Ali Reza (University of Sistan and Baluchestan. Department of Chemistry)
One new lead(II) coordination supramolecular complex (CSC) (1D), [Pb(L)(I)], L = CHN (1-methyl imidazole), has been synthesized under different experimental conditions. Micrometric crystals (bulk) or nano-sized materials have been obtained depending on using the branch tube method or sonochemical irradiation. [...]
2018 - 10.1016/j.ultsonch.2017.11.033
Ultrasonics sonochemistry, Vol. 42 (April 2018) , p. 320-326
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27 p, 1.3 MB |
Delamination of 2D coordination polymers : the role of solvent and ultrasound
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Contreras Pereda, Noemí (Institut Català de Nanociència i Nanotecnologia) ;
Hayati, Payam (Institut Català de Nanociència i Nanotecnologia) ;
Suárez García, Salvio (Institut Català de Nanociència i Nanotecnologia) ;
Esrafili, L. (Tarbiat Modares University. Department of Chemistry) ;
Retailleau, Pascal (Institut de chimie des substances naturelles) ;
Benmansour Souilamas, Samia (Universitat de València. Institut de Ciència dels Materials) ;
Novio Vázquez, Fernando (Institut Català de Nanociència i Nanotecnologia) ;
Morsali, Ali (Tarbiat Modares University. Department of Chemistry) ;
Ruiz-Molina, Daniel (Institut Català de Nanociència i Nanotecnologia)
Two novel cadmium-based 2D coordination polymers have been synthesized and characterized. Experimental results evidence that the best delamination processes occurs when weak interactions dominate the cohesion between layers and solvent molecules are occluded within the crystalline network. [...]
2019 - 10.1016/j.ultsonch.2019.02.014
Ultrasonics sonochemistry, Vol. 55 (July 2019) , p. 186-195
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11 p, 1.2 MB |
Influence of the Amide Groups in the CO2/N2 Selectivity of a Series of Isoreticular, Interpenetrated Metal-Organic Frameworks
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Safarifard, Vahid (Institut Català de Nanociència i Nanotecnologia) ;
Rodríguez-Hermida, Sabina (Institut Català de Nanociència i Nanotecnologia) ;
Guillerm, Vincent (Institut Català de Nanociència i Nanotecnologia) ;
Imaz, Inhar (Institut Català de Nanociència i Nanotecnologia) ;
Bigdeli, Mina (Tarbiat Modares University. Department of Chemistry) ;
Tehrani, Alireza Azhdari (Tarbiat Modares University. Department of Chemistry) ;
Juanhuix, Judith (ALBA Laboratori de Llum de Sincrotró) ;
Morsali, Ali (Tarbiat Modares University. Department of Chemistry) ;
Casco, Mirian E. (Universitat d'Alacant. Departament de Química Inorgànica) ;
Silvestre Albero, Joaquín (Universitat d'Alacant. Departament de Química Inorgànica) ;
Ramos Fernández, Enrique V. (Universitat d'Alacant. Departament de Química Inorgànica) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia)
Here we report the use of a pillaring strategy for the design and synthesis of three novel amide-functionalized metal-organic frameworks (MOFs), TMUs-22/-23/-24, isoreticular to the recently reported imine-functionalized TMU-6 and TMU-21 MOFs. [...]
2016 - 10.1021/acs.cgd.6b01054
Crystal Growth and Design, Vol. 16, Issue 10 (October 2016) , p. 6016-6023
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