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12 p, 1.6 MB |
How reproducible are surface areas calculated from the BET equation?
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Osterrieth, Johannes W. M. (University of Cambridge. Department of Chemical Engineering & Biotechnology) ;
Rampersad, James (University of Cambridge. Department of Chemical Engineering & Biotechnology) ;
Madden, David (University of Cambridge. Department of Chemical Engineering & Biotechnology) ;
Rampal, Nakul (University of Cambridge. Department of Chemical Engineering & Biotechnology) ;
Skoric, Luka (University of Cambridge. Cavendish Laboratory) ;
Connolly, Bethany (University of Cambridge. Department of Chemical Engineering & Biotechnology) ;
Allendorf, Mark D. (Sandia National Laboratories) ;
Stavila, Vitalie (Sandia National Laboratories) ;
Snider, Jonathan L. (Sandia National Laboratories) ;
Ameloot, Rob (KU Leuven. Department of Microbial and Molecular Systems) ;
Marreiros, João (KU Leuven. Department of Microbial and Molecular Systems) ;
Ania, Conchi (Université d'Orléans) ;
Azevedo, Diana (Federal University of Ceará. Department of Chemical Engineering) ;
Vilarrasa-Garcia, E. (Federal University of Ceará. Department of Chemical Engineering) ;
Santos, Bianca F. (Federal University of Ceará. Department of Chemical Engineering) ;
Bu, Xian-He (Nankai University. School of Materials Science and Engineering) ;
Chang, Ze (Nankai University. School of Materials Science and Engineering) ;
Bunzen, Hana (University of Augsburg. Institute of Physics) ;
Champness, Neil (University of Nottingham. School of Chemistry) ;
Griffin, Sarah (University of Nottingham. School of Chemistry) ;
Chen, Banglin (University of Texas at San Antonio. Department of Chemistry) ;
Lin, Rui-Biao (University of Texas at San Antonio. Department of Chemistry) ;
Coasne, Benoit (Université Grenoble Alpes) ;
Cohen, Seth (University of California. Department of Chemistry and Biochemistry) ;
Moreton, Jessica C. (University of California. Department of Chemistry and Biochemistry) ;
Colón, Yamil J. (Université de Nôtre Dame) ;
Chen, Linjiang (Leverhulme Research Centre for Functional Materials Design) ;
Clowes, Rob (Leverhulme Research Centre for Functional Materials Design) ;
Coudert, François-Xavier (Chimie ParisTech) ;
Cui, Yong (Shanghai Jiaotong University. School of Chemistry and Chemical Engineering) ;
Hou, Bang (Shanghai Jiaotong University. School of Chemistry and Chemical Engineering) ;
D'Alessandro, Deanna M. (The University of Sydney. School of Chemistry) ;
Doheny, Patrick W. (The University of Sydney. School of Chemistry) ;
Dincă, Mircea (Massachusetts Institute of Technology. Department of Chemistry) ;
Sun, Chenyue (Massachusetts Institute of Technology. Department of Chemistry) ;
Doonan, Christian (The University of Adelaide. Centre for Advanced Nanomaterials and Department of Chemistry) ;
Huxley, Michael Thomas (The University of Adelaide. Centre for Advanced Nanomaterials and Department of Chemistry) ;
Evans, Jack D. (Technische Universität Dresden. Department of Inorganic Chemistry) ;
Falcaro, Paolo (Graz University of Technology. Institute of Physical and Theoretical Chemistry) ;
Riccò, Raffaele (Graz University of Technology. Institute of Physical and Theoretical Chemistry) ;
Farha, Omar (Northwestern University. Department of Chemistry) ;
Idrees, Karam B. (Northwestern University. Department of Chemistry) ;
Islamoglu, Timur (Northwestern University. Department of Chemistry) ;
Feng, Pingyun (University of California. Department of Chemistry) ;
Yang, Huajun (University of California. Department of Chemistry) ;
Forgan, Ross (University of Glasgow. School of Chemistry) ;
Bara, Dominic (University of Glasgow. School of Chemistry) ;
Furukawa, Shuhei (Kyoto University. Institute for Integrated Cell-Material Sciences) ;
Sanchez, Eli (Kyoto University. Institute for Integrated Cell-Material Sciences) ;
Gascon, Jorge (KAUST Catalysis Center) ;
Telalović, Selvedin (KAUST Catalysis Center) ;
Ghosh, Sujit K. (Indian Institute of Science Education and Research. Department of Chemistry) ;
Mukherjee, Soumya (Indian Institute of Science Education and Research. Department of Chemistry) ;
Hill, Matthew R. (Monash University. Department of Chemical Engineering) ;
Sadiq, Muhammed Munir (Monash University. Department of Chemical Engineering) ;
Horcajada, Patricia (IMDEA Energy) ;
Salcedo-Abraira, Pablo (IMDEA Energy) ;
Kaneko, Katsumi (Shinshu University. Research Initiative for Supra-Materials) ;
Kukobat, Radovan (Shinshu University. Research Initiative for Supra-Materials) ;
Kenvin, Jeff (Micromeritics Instrument Corporation) ;
Keskin, Seda (Koc University. Department of Chemical and Biological Engineering) ;
Kitagawa, Susumu (Kyoto University Institute for Advanced Study) ;
Otake, Ken-ichi (Kyoto University Institute for Advanced Study) ;
Lively, Ryan P. (Georgia Institute of Technology. School of Chemical & Biomolecular Engineering) ;
DeWitt, Stephen J.A. (Georgia Institute of Technology. School of Chemical & Biomolecular Engineering) ;
Llewellyn, Phillip (CNRS / Aix-Marseille Univ./Total) ;
Lotsch, Bettina V. (University of Munich. Department of Chemistry) ;
Emmerling, Sebastian T. (University of Munich. Department of Chemistry) ;
Pütz, Alexander M. (University of Munich. Department of Chemistry) ;
Martí-Gastaldo, Carlos (Universitat de València. Instituto de Ciencia Molecular) ;
Padial, Natalia M. (Universitat de València. Instituto de Ciencia Molecular) ;
Garcia-Martinez, Javier (Universitat d'Alacant. Laboratori de Nanotecnologia Molecular) ;
Linares, Noemi (Universitat d'Alacant. Laboratori de Nanotecnologia Molecular) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia) ;
Suárez del Pino, José A. (Institut Català de Nanociència i Nanotecnologia) ;
Moghadam, Peyman (The University of Sheffield. Department of Chemical and Biological Engineering) ;
Oktavian, Rama (The University of Sheffield. Department of Chemical and Biological Engineering) ;
Morris, Russel E. (University of St Andrews. School of Chemistry) ;
Wheatley, Paul S. (University of St Andrews. School of Chemistry) ;
Navarro, Jorge (Universidad de Granada) ;
Petit, Camille (Barrer Centre) ;
Danaci, David (Barrer Centre) ;
Rosseinsky, Matthew J. (University of Liverpool. Department of Chemistry) ;
Katsoulidis, Alexandros P. (University of Liverpool. Department of Chemistry) ;
Schröder, Martin (The University of Manchester. School of Chemistry) ;
Han, Xue (The University of Manchester. School of Chemistry) ;
Yang, Sihai (The University of Manchester. School of Chemistry) ;
Serre, Christian (Institut des Matériaux Poreux de Paris) ;
Mouchaham, Georges (Institut des Matériaux Poreux de Paris) ;
Sholl, David S. (Georgia Institute of Technology. School of Chemical & Biomolecular Engineering) ;
Thyagarajan, Raghuram (Georgia Institute of Technology. School of Chemical & Biomolecular Engineering) ;
Siderius, Daniel W. (Chemical Sciences Division. National Institute of Standards and Technology) ;
Snurr, Randall Q. (Northwestern University. Department of Chemical & Biological Engineering) ;
Barbosa Goncalves, Rebecca (Northwestern University. Department of Chemistry) ;
Telfer, Shane (MacDiarmid Institute for Advanced Materials and Nanotechnology) ;
Lee, Seok J. (MacDiarmid Institute for Advanced Materials and Nanotechnology) ;
Ting, V.P. (University of Bristol. Department of Mechanical Engineering) ;
Rowlandson, Jemma L. (University of Bristol. Department of Mechanical Engineering) ;
Uemura, Takashi (The University of Tokyo. Department of Advanced Materials Science) ;
Iiyuka, Tomoya (The University of Tokyo. Department of Advanced Materials Science) ;
van der Veen, Monique (Delft University of Technology. Department of Chemical Engineering) ;
Rega, Davide (Delft University of Technology. Department of Chemical Engineering) ;
Van Speybroeck, Veronique (Ghent University. Center for Molecular Modeling) ;
Rogge, Sven M.J. (Ghent University. Center for Molecular Modeling) ;
Lamaire, Aran (Ghent University. Center for Molecular Modeling) ;
Walton, Krista S. (Georgia Institute of Technology. School of Chemical & Biomolecular Engineering) ;
Bingel, Lukas (Georgia Institute of Technology. School of Chemical & Biomolecular Engineering) ;
Wuttke, Stefan (IKERBASQUE) ;
Andreo, Jacopo (IKERBASQUE) ;
Yaghi, Omar M. (Berkeley Global Science Institute) ;
Zhang, Bing (University of California. Department of Chemistry) ;
Yavuz, Cafer Tayyar (Korea Advanced Institute of Science and Technology) ;
Nguyen, Thien S. (Korea Advanced Institute of Science and Technology) ;
Zamora, Félix (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ;
Montoro, Carmen (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ;
Zhou, Hongcai (Texas A&M University. Department of Chemistry) ;
Kirchon, Angelo (Texas A&M University. Department of Chemistry) ;
Fairen-Jimenez, David (University of Cambridge. Department of Chemical Engineering & Biotechnology)
Porosity and surface area analysis play a prominent role in modern materials science. At the heart of this sits the Brunauer-Emmett-Teller (BET) theory, which has been a remarkably successful contribution to the field of materials science. [...]
2022 -  10.1002/adma.202201502
Advanced materials, Vol. 34, issue 27 (July 2022) , art. 2201502
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2.
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9 p, 2.6 MB |
Ultralarge Free-Standing Imine-Based Covalent Organic Framework Membranes Fabricated via Compression
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Martín-Illán, Jesús Á. (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ;
Suárez, José Antonio (Institut Català de Nanociència i Nanotecnologia) ;
Gómez-Herrero, Julio (Universidad Autónoma de Madrid. Departamento de Física de la Materia Condensada) ;
Ares, Pablo (Universidad Autónoma de Madrid. Departamento de Física de la Materia Condensada) ;
Gallego-Fuente, Daniel (Universidad Autónoma de Madrid. Departamento de Física de la Materia Condensada) ;
Cheng, Youdong (National University of Singapore) ;
Zhao, Dan (National University of Singapore) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia) ;
Zamora, Félix (Universidad Autónoma de Madrid. Departamento de Química Inorgánica)
Demand continues for processing methods to shape covalent organic frameworks (COFs) into macroscopic objects that are needed for their practical applications. Herein, a simple compression method to prepare large-scale, free-standing homogeneous and porous imine-based COF-membranes with dimensions in the centimeter range and excellent mechanical properties is reported. [...]
2022 - 10.1002/advs.202104643
Advanced science, Vol. 9, Issue 7 (March 2022) , art. 2104643
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3.
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20 p, 1.7 MB |
Biomimetic synthesis of sub-20 nm covalent organic frameworks in water
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Franco, Carlos (ETH Zurich. Department of Chemistry and Applied Biosciences) ;
Rodríguez-San-Miguel, David (Universidad Autónoma de Madrid. Instituto de Física de la Materia Condensada-IFIMAC) ;
Sorrenti, Alessandro (ETH Zurich. Department of Chemistry and Applied Biosciences) ;
Sevim, Semih (ETH Zurich. Department of Chemistry and Applied Biosciences) ;
Pons, Ramon (Institut de Química Avançada de Catalunya) ;
Platero-Prats, Ana Eva (Universidad Autónoma de Madrid. Instituto de Física de la Materia Condensada-IFIMAC) ;
Pavlovic, Marko (Max-Planck Institute of Colloids and Interfaces. Department of Colloid Chemistry) ;
Szilágyi, Istvan (University of Szeged. Department of Physical Chemistry and Materials Science) ;
Ruiz Gonzalez, M. Luisa (Universidad Complutense de Madrid. Departamento de Química Inorgánica) ;
González-Calbet, José M. (Universidad Complutense de Madrid. Departamento de Química Inorgánica) ;
Bochicchio, Davide (University of Applied Sciences and Arts of Southern Switzerland. Department of Innovative Technologies) ;
Pesce, Luca (University of Applied Sciences and Arts of Southern Switzerland. Department of Innovative Technologies) ;
Pavan, Giovanni M. (University of Applied Sciences and Arts of Southern Switzerland. Department of Innovative Technologies) ;
Imaz, Inhar (Institut Català de Nanociència i Nanotecnologia) ;
Cano-Sarabia, Mary (Institut Català de Nanociència i Nanotecnologia) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia) ;
Pané i Vidal, Salvador (ETH Zurich. Multi-Scale Robotics Lab) ;
De Mello, Andrew J. (ETH Zurich. Department of Chemistry and Applied Biosciences) ;
Zamora, Félix (Universidad Autónoma de Madrid. Instituto de Física de la Materia Condensada-IFIMAC) ;
Puigmarti-Luis, Josep (ETH Zurich. Department of Chemistry and Applied Biosciences)
Covalent organic frameworks (COFs) are commonly synthesized under harsh conditions yielding unprocessable powders. Control in their crystallization process and growth has been limited to studies conducted in hazardous organic solvents. [...]
2020 - 10.1021/jacs.9b12389
Journal of the American Chemical Society, Vol. 142, issue 7 (Feb. 2020) , p. 3540-3547
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6 p, 552.4 KB |
Green synthesis of imine-based covalent organic frameworks in water
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Martín-Illán, Jesús A. (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ;
Rodríguez-San-Miguel, David (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ;
Franco, Carlos (ETH Zurich. Department of Chemistry and Applied Biosciences) ;
Imaz, Inhar (Institut Català de Nanociència i Nanotecnologia) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia) ;
Puigmarti-Luis, Josep (ETH Zurich. Department of Chemistry and Applied Biosciences) ;
Zamora, Félix (Instituto Madrileño de Estudios Avanzados en Nanociencia)
Dynamic covalent bonds have been advantageously used to direct the synthesis of crystalline porous covalent organic frameworks (COFs). Unlike the standard synthetic protocols that involve harsh conditions, this work provides a high-yield "one-pot"green synthesis of imine-based COFs in water. [...]
2020 - 10.1039/d0cc02033h
Chemical communications, Vol. 56, issue 49 (June 2020) , p. 6704-6707
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5.
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7 p, 804.7 KB |
Confining Functional Nanoparticles into Colloidal Imine-Based COF Spheres by a Sequential Encapsulation-Crystallization Method
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Rodríguez-San-Miguel, David (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ;
Yazdi, Amirali (Institut Català de Nanociència i Nanotecnologia) ;
Guillerm, Vincent (Institut Català de Nanociència i Nanotecnologia) ;
Pérez-Carvajal, Javier (Institut Català de Nanociència i Nanotecnologia) ;
Puntes, Víctor (Institut Català de Nanociència i Nanotecnologia) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia) ;
Zamora, Félix (Universidad Autónoma de Madrid. Departamento de Química Inorgánica)
Here, a two-step method is reported that enables imparting new functionalities to covalent organic frameworks (COFs) by nanoparticle confinement. The direct reaction between 1,3,5-tris(4-aminophenyl)benzene and 1,3,5-benzenetricarbaldehyde in the presence of a variety of metallic/metal-oxide nanoparticles resulted in embedding of the nanoparticles in amorphous and non-porous imine-linked polymer organic spheres (NP@a-1). [...]
2017 - 10.1002/chem.201702072
Chemistry, Vol. 23, Issue 36 (June 2017) , p. 8623-8627
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7 p, 661.1 KB |
A MOF@COF Composite with Enhanced Uptake through Interfacial Pore Generation
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Garzon-Tovar, Luis (Institut Català de Nanociència i Nanotecnologia) ;
Pérez-Carvajal, Javier (Institut Català de Nanociència i Nanotecnologia) ;
Yazdi, Amirali (Institut Català de Nanociència i Nanotecnologia) ;
Hernández Muñoz, José (Universidad Autónoma de Madrid. Departamento de Física Teórica de la Materia Condensada) ;
Tarazona, Pedro (Universidad Autónoma de Madrid. Departamento de Física Teórica de la Materia Condensada) ;
Imaz, Inhar (Institut Català de Nanociència i Nanotecnologia) ;
Zamora, Félix (Instituto Madrileño de Estudios Avanzados en Nanociencia) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia)
Herein, we describe a new class of porous composites comprising metal-organic framework (MOF) crystals confined in single spherical matrices made of packed covalent-organic framework (COF) nanocrystals. [...]
2019 - 10.1002/anie.201904766
Angewandte Chemie (International ed. Internet), Vol. 58, Issue 28 (July 2019) , p. 9512-9516
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19 p, 689.5 KB |
Reversible thermochromic polymeric thin films made of ultrathin 2D crystals of coordination polymers based on copper(I)-thiophenolates
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Troyano, Javier (Institut Català de Nanociència i Nanotecnologia) ;
Castillo, Óscar. (Universidad del País Vasco. Departamento de Química Inorgánica) ;
Martínez, José I. (Instituto de Ciencia de Materiales de Madrid) ;
Fernández-Moreira, Vanesa (Universidad de Zaragoza. Departamento de Química Inorgánica) ;
Ballesteros, Yolanda (Universidad Pontificia Comillas. Departamento de Ingeniería Mecánica) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia) ;
Zamora, Félix (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ;
Delgado, Salomé (Universidad Autónoma de Madrid. Departamento de Química Inorgánica)
A one-pot reaction between Cu(BF)·xHO and 4-mercaptobenzoic acid in acetone or methanol gives rise to the formation of lamellar microcrystals of two Cu(I)-thiophenolate-based coordination polymers (CPs) with the formulas [CuCT] (1) (CT = 4-carboxy-thiophenolate) and [CuMCT] (2) (MCT = 4-methoxycarbonyl-thiophenolate). [...]
2018 - 10.1002/adfm.201704040
Advanced functional materials, Vol. 28, issue 5 (Jan. 2018) , art. 1704040
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5 p, 626.4 KB |
Spray drying for making covalent chemistry II : synthesis of covalent-organic framework superstructures and related composites
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Garzon-Tovar, Luis (Institut Català de Nanociència i Nanotecnologia) ;
Camur, Ceren (Institut Català de Nanociència i Nanotecnologia) ;
Rodríguez-San-Miguel, David (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ;
Imaz, Inhar (Institut Català de Nanociència i Nanotecnologia) ;
Zamora, Félix (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ;
Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia)
Here we report a method that combines the spray-drying technique with a dynamic covalent chemistry process to synthesize zero-dimensional, spherical and microscale superstructures made from the assembly of imine-based COF nanocrystals. [...]
2017 - 10.1039/c7cc07052g
Chemical communications, Vol. 53, issue 82 (Oct. 2017) , p. 11372-11375
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