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1.
9 p, 1.6 MB Synthesis of 2D porous crystalline materials in simulated microgravity / Contreras Pereda, Noemí (Institut Català de Nanociència i Nanotecnologia) ; Rodríguez-San-Miguel, David (Institut de Química Teòrica i Computacional. Departament de Ciència dels Materials i Química Física) ; Franco, Carlos (Eidgenössische Technische Hochschule Zürich. Department of Chemistry and Applied Biosciences) ; Sevim, Semih (Eidgenössische Technische Hochschule Zürich. Department of Chemistry and Applied Biosciences) ; Vale, Joao Pedro (SIMTECH Lab) ; Solano, Eduardo (ALBA Laboratori de Llum de Sincrotró) ; Fong, Wye-Khay (University of Newcastle. School of Environmental and Life Sciences) ; Del Giudice, Alessandra (Università degli studi di Roma "La Sapienza". Department of Chemistry) ; Galantini, Luciano (Department of Chemistry. Sapienza University of Rome) ; Pfattner, Raphael (Institut de Ciència de Materials de Barcelona) ; Pané i Vidal, Salvador (Eidgenössische Technische Hochschule Zürich. Multi-Scale Robotics Lab) ; Sotto Mayor, Tiago. (SIMTECH Lab) ; Ruiz-Molina, Daniel (Institut Català de Nanociència i Nanotecnologia) ; Puigmartí-Luis, Josep (Institució Catalana de Recerca i Estudis Avançats)
To date, crystallization studies conducted in space laboratories, which are prohibitively costly and unsuitable to most research laboratories, have shown the valuable effects of microgravity during crystal growth and morphogenesis. [...]
2021 - 10.1002/adma.202101777
Advanced materials, Vol. 33, issue 30 (July 2021) , art. 2101777  
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2.
20 p, 1.7 MB Biomimetic synthesis of sub-20 nm covalent organic frameworks in water / Franco, Carlos (ETH Zurich. Department of Chemistry and Applied Biosciences) ; Rodríguez-San-Miguel, David (Universidad Autónoma de Madrid. Instituto de Física de la Materia Condensada-IFIMAC) ; Sorrenti, Alessandro (ETH Zurich. Department of Chemistry and Applied Biosciences) ; Sevim, Semih (ETH Zurich. Department of Chemistry and Applied Biosciences) ; Pons, Ramon (Institut de Química Avançada de Catalunya) ; Platero-Prats, Ana Eva (Universidad Autónoma de Madrid. Instituto de Física de la Materia Condensada-IFIMAC) ; Pavlovic, Marko (Max-Planck Institute of Colloids and Interfaces. Department of Colloid Chemistry) ; Szilágyi, Istvan (University of Szeged. Department of Physical Chemistry and Materials Science) ; Ruiz Gonzalez, M. Luisa (Universidad Complutense de Madrid. Departamento de Química Inorgánica) ; González-Calbet, José M. (Universidad Complutense de Madrid. Departamento de Química Inorgánica) ; Bochicchio, Davide (University of Applied Sciences and Arts of Southern Switzerland. Department of Innovative Technologies) ; Pesce, Luca (University of Applied Sciences and Arts of Southern Switzerland. Department of Innovative Technologies) ; Pavan, Giovanni M. (University of Applied Sciences and Arts of Southern Switzerland. Department of Innovative Technologies) ; Imaz, Inhar (Institut Català de Nanociència i Nanotecnologia) ; Cano-Sarabia, Mary (Institut Català de Nanociència i Nanotecnologia) ; Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia) ; Pané i Vidal, Salvador (ETH Zurich. Multi-Scale Robotics Lab) ; De Mello, Andrew J. (ETH Zurich. Department of Chemistry and Applied Biosciences) ; Zamora, Félix (Universidad Autónoma de Madrid. Instituto de Física de la Materia Condensada-IFIMAC) ; Puigmarti-Luis, Josep (ETH Zurich. Department of Chemistry and Applied Biosciences)
Covalent organic frameworks (COFs) are commonly synthesized under harsh conditions yielding unprocessable powders. Control in their crystallization process and growth has been limited to studies conducted in hazardous organic solvents. [...]
2020 - 10.1021/jacs.9b12389
Journal of the American Chemical Society, Vol. 142, issue 7 (Feb. 2020) , p. 3540-3547  
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3.
6 p, 552.4 KB Green synthesis of imine-based covalent organic frameworks in water / Martín-Illán, Jesús A. (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ; Rodríguez-San-Miguel, David (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ; Franco, Carlos (ETH Zurich. Department of Chemistry and Applied Biosciences) ; Imaz, Inhar (Institut Català de Nanociència i Nanotecnologia) ; Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia) ; Puigmarti-Luis, Josep (ETH Zurich. Department of Chemistry and Applied Biosciences) ; Zamora, Félix (Instituto Madrileño de Estudios Avanzados en Nanociencia)
Dynamic covalent bonds have been advantageously used to direct the synthesis of crystalline porous covalent organic frameworks (COFs). Unlike the standard synthetic protocols that involve harsh conditions, this work provides a high-yield "one-pot"green synthesis of imine-based COFs in water. [...]
2020 - 10.1039/d0cc02033h
Chemical communications, Vol. 56, issue 49 (June 2020) , p. 6704-6707  
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4.
7 p, 804.7 KB Confining Functional Nanoparticles into Colloidal Imine-Based COF Spheres by a Sequential Encapsulation-Crystallization Method / Rodríguez-San-Miguel, David (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ; Yazdi, Amirali (Institut Català de Nanociència i Nanotecnologia) ; Guillerm, Vincent (Institut Català de Nanociència i Nanotecnologia) ; Pérez-Carvajal, Javier (Institut Català de Nanociència i Nanotecnologia) ; Puntes, Víctor (Institut Català de Nanociència i Nanotecnologia) ; Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia) ; Zamora, Félix (Universidad Autónoma de Madrid. Departamento de Química Inorgánica)
Here, a two-step method is reported that enables imparting new functionalities to covalent organic frameworks (COFs) by nanoparticle confinement. The direct reaction between 1,3,5-tris(4-aminophenyl)benzene and 1,3,5-benzenetricarbaldehyde in the presence of a variety of metallic/metal-oxide nanoparticles resulted in embedding of the nanoparticles in amorphous and non-porous imine-linked polymer organic spheres (NP@a-1). [...]
2017 - 10.1002/chem.201702072
Chemistry, Vol. 23, Issue 36 (June 2017) , p. 8623-8627  
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5.
5 p, 626.4 KB Spray drying for making covalent chemistry II : synthesis of covalent-organic framework superstructures and related composites / Garzon-Tovar, Luis (Institut Català de Nanociència i Nanotecnologia) ; Camur, Ceren (Institut Català de Nanociència i Nanotecnologia) ; Rodríguez-San-Miguel, David (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ; Imaz, Inhar (Institut Català de Nanociència i Nanotecnologia) ; Zamora, Félix (Universidad Autónoma de Madrid. Departamento de Química Inorgánica) ; Maspoch Comamala, Daniel (Institut Català de Nanociència i Nanotecnologia)
Here we report a method that combines the spray-drying technique with a dynamic covalent chemistry process to synthesize zero-dimensional, spherical and microscale superstructures made from the assembly of imine-based COF nanocrystals. [...]
2017 - 10.1039/c7cc07052g
Chemical communications, Vol. 53, issue 82 (Oct. 2017) , p. 11372-11375
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