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Synthesis and characterization of a new nano lead(II) 0-D coordination supramolecular compound : a precursor to produce pure phase nano-sized lead(II) oxide
Fard, Mohammad Jaafar Soltanian (Islamic Azad University. Department of Chemistry)
Hayati, Payam (Institut Català de Nanociència i Nanotecnologia)
Naraghi, Hakimeh Sadat (Islamic Azad University. Department of Chemistry)
Tabeie, Sayed Abbas (Islamic Azad University. Department of Chemistry)

Date: 2017
Abstract: Nano-structure of a new 0D Pb(II) coordination supramolecular compound, [Pb(8-Quin)](ClO)(1), L = 8-HQuin = 8-hydroxyquinolin ligand has been synthesized by use of a sonochemical process and characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRPD), Fourier transform infrared spectroscopy (FTIR) and elemental analyses. The structure of compound 1 was determined by single-crystal X-ray diffraction. The single crystal X-ray data of compound 1 implies that the Pb ions are five coordinated. Each lead atom is coordinated to nitrogen and oxygen atoms of 8-hydroxyquinolin ligand. Topological analysis shows that the compound 1 is 1,2,3,4,4M12-1net. Nanoparticles of lead(II) oxide have been prepared by calcination of lead(II) coordination polymer at 500 °C that were characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRPD) and IR spectroscopy.
Rights: Aquest document està subjecte a una llicència d'ús Creative Commons. Es permet la reproducció total o parcial, la distribució, i la comunicació pública de l'obra, sempre que no sigui amb finalitats comercials, i sempre que es reconegui l'autoria de l'obra original. No es permet la creació d'obres derivades. Creative Commons
Language: Anglès
Document: article ; recerca ; acceptedVersion
Subject: Nanoparticles ; Lead(II) oxide ; Coordination supramolecular ; Ultrasonic
Published in: Ultrasonics sonochemistry, Vol. 39 (November 2017) , p. 129-136, ISSN 1873-2828

DOI: 10.1016/j.ultsonch.2017.04.023


Postprint
34 p, 991.8 KB

The record appears in these collections:
Research literature > UAB research groups literature > Research Centres and Groups (scientific output) > Experimental sciences > Catalan Institute of Nanoscience and Nanotechnology (ICN2)
Articles > Research articles
Articles > Published articles

 Record created 2020-06-25, last modified 2020-08-30



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