Web of Science: 28 citations, Scopus: 31 citations, Google Scholar: citations,
Scalable Heating-Up Synthesis of Monodisperse Cu2ZnSnS4 Nanocrystals
Shavel, Alexey (Institut de Recerca en Energia de Catalunya)
Ibáñez, Maria (Institut de Recerca en Energia de Catalunya)
Luo, Zhishan (Institut de Recerca en Energia de Catalunya)
De Roo, Jonathan (Ghent University. Department of Inorganic and Physical Chemistry)
Carrete, Alex (Institut de Recerca en Energia de Catalunya)
Dimitrievska, Mirjana (Institut de Recerca en Energia de Catalunya)
Genç, Aziz (Institut Català de Nanociència i Nanotecnologia)
Meyns, Michaela (Institut de Recerca en Energia de Catalunya)
Pérez-Rodríguez, Alejandro (Institut de Recerca en Energia de Catalunya)
Kovalenko, Maksym V. (Institute of Inorganic Chemistry (Bratislava, Eslovàquia))
Arbiol i Cobos, Jordi (Institut Català de Nanociència i Nanotecnologia)
Cabot, Andreu (Institut de Recerca en Energia de Catalunya)

Date: 2016
Abstract: Monodisperse CuZnSnS (CZTS) nanocrystals (NCs), with quasi-spherical shape, were prepared by a facile, high-yield, scalable, and high-concentration heat-up procedure. The key parameters to minimize the NC size distribution were efficient mixing and heat transfer in the reaction mixture through intensive argon bubbling and improved control of the heating ramp stability. Optimized synthetic conditions allowed the production of several grams of highly monodisperse CZTS NCs per batch, with up to 5wt% concentration in a crude solution and a yield above 90%.
Note: Número d'acord de subvenció EC/FP7/310250
Note: Número d'acord de subvenció EC/FP7/284486
Note: Número d'acord de subvenció EC/FP7/316488
Note: Número d'acord de subvenció MINECO/ENE2013-46624-C4-3-R
Note: Número d'acord de subvenció AGAUR/2013/BP-A00344
Note: Número d'acord de subvenció AGAUR/2014/SGR-1638
Note: Número d'acord de subvenció EC/FP7/306733
Rights: Tots els drets reservats
Language: Anglès.
Document: article ; recerca ; acceptedVersion
Subject: Heating ramps ; High yield ; Improved controls ; Mono-disperse ; Nanocrystal (NCs) ; Reaction mixture ; Spherical shape ; Synthetic conditions
Published in: Chemistry of Materials, Vol. 28, Núm. 3 (February 2016) , p. 720-726, ISSN 1520-5002

DOI: 10.1021/acs.chemmater.5b03417


Post-print
9 p, 2.1 MB

The record appears in these collections:
Research literature > UAB research groups literature > Research Centres and Groups (scientific output) > Experimental sciences > Catalan Institute of Nanoscience and Nanotechnology (ICN2)
Articles > Research articles
Articles > Published articles

 Record created 2018-09-18, last modified 2019-12-18



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