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6 p, 2.0 MB Palladium-Catalyzed Ortho C-H Arylation of Unprotected Anilines : Chemo- and Regioselectivity Enabled by the Cooperating Ligand [2,2'-Bipyridin]-6(1 H)-one / Pinilla, Cintya (Universidad de Valladolid) ; Salamanca, Vanesa (Universidad de Valladolid) ; Lledós, Agustí (Universitat Autònoma de Barcelona. Departament de Química) ; Albéniz, Ana C. (Universidad de Valladolid)
Metal-catalyzed C-H functionalizations on the aryl ring of anilines usually need cumbersome N-protection-deprotection strategies to ensure chemoselectivity. We describe here the Pd-catalyzed direct C-H arylation of unprotected anilines with no competition of the N-arylation product. [...]
2022 - 10.1021/acscatal.2c05206
ACS catalysis, Vol. 12, Núm. 23 (November 2022) , p. 14527-14532  
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